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GCMS analysis results, sample AE09974, May 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE09974 showing surrogate recovery and unknown compounds from May 9, 2002.

NYC-WTC_000044055–000044070

Folder label: “GCMS X 4/25/02 A 5/7/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050602\9974 .D Vial: 22 Acq On 7 May 2002 4:48 am Operator: Mclean Sample 4/25 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 2 Anthracene, 9-methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.36 ug/L 410728 Phenanthranene -dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene, 9-methyl- 192 C15H12 000779-02-2 59 2 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 59 3 Anthracene, 9-methyl- 192 C15H12 000779-02-2 53 4 1H-Indene, 2-phenyl- 192 C15H12 004505-48-0 45 Abundance Scan 3319 (22.580 min): 9974. D (-3312) (-) m/z 192.10 100.00% 192

5000

o 1 46 1 1 1 1 ' 11 1 1 1 1 1 1 1 22.20 22.40 22.60 22.80 23.00 42 52 70 82 J 120 | 160 | — I I I I I I I I I I I I I mfui I I I I I I I I I I I I I I I I I I'l I m I I I I I I I I > I j I I I I I I rP I I I I I 'I I I I I I I I I I I I I I I I m/ z 191.10 17.19% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125848: Anthracene, 9-methyl- 192

5000 n 22.20 22.40 22.60 22.80 23.00 i 1 1 ' * i 1

m/z 146.10 15.86% 96 EE m/z-> 27 39 51 63 82 J 115 126 1391 I ।152 । | । > । । | । । r r‘| i i i 1 17 । I । । | i’i i । । I'l । pl i I'I'] 1 II I "j । li । jiii । | । । ' । |"l'l I'l

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 pl I I I ° 176 I | ill 1 | r ri'I | I 4 TTTT

Abundance #81033: Phenanthrene, 9-methyl- 192 -------------------------- 22.20 22.40 22.60 22.80 23.00 5000 "z 193.10 14.63%

96 165 i i 29 39 51 63 74 83 J 115 126 139 152 । 176 | 1 । । । । ' । । 1 1 i| r 1 । • । r > 1 1 । 1' 1 i 1 । i r i 1 |‘I । rl| ill IIIII I"I"I"I"M*I । i i i । i i i "FUTI r pt III i'l i i | i rli | ri i'l 11 III m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125849: Anthracene, 9-methyl- ' ‘ I ' ' 1 ' I ' 192 22.20 22.40 22.60 22.80 23.00 m/z 96.00 12.27% 5000

_ 96 165 28 39 51 63 74 83 J 105 115 126 139 152 J 176 TT 1 1 lg < 1 i' | 1 1 1 । ]'1 r i r [ I 'l I 1 | > I' I i |' ।' । I’lT l| I r r i r'ti i rrri [' I I ) I '| I I I I |11 I I I [ '1 t ! I pr I'll | | | | I ‘ I 11’’’’ I’’ 1 1 i 1 ■ 1 1 i 1 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00

9974.D 050102.M Tue May 07 15:53:28 2002 Page 6

NYC-WTC_000044065

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