GCMS sample analysis results for AE10603, May 10 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050702\10603 .D Vial: 8 Acq On 7 May 2002 6:50 pm Operator: Mclean Sample 5/3 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L Peak Number 6 Phenanthrene, 9-methyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 22.58 0.34 ug/L 462520 Phenanthranene-dl0 22.96 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 2 Anthracene, 9-methyl- 192 C15H12 000779-02-2 42 3 Anthracene, 9-methyl- 192 C15H12 000779-02-2 42 4 Phenanthrene, 3-methyl- 192 C15H12 000832-71-342 Abundance Scan 3319 (22.580 min): 10603. D (-3309) (-) m/z 192.10 100.00% 192

5000

82 9,6 146 160 l I I I I I I I I I I .... A I Til I 1 I I I I I I I

m/z-> 42 52 70 । I' H i p I I' । । । । । 118 T T r r IT —TH I I | I I I I ] I t f I | I I I I I | | f r I [ i I i i | 1 । 1111 ri' । । k 1111111111111 h 111 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 H 22.20 22.40 22.60 22.80 23.00 m/z 191.10 19.44% Abundance #81033: Phenanthrene, 9-methyl- 192

5000 I I I I I I I 1 I I 1 I I l l l > ( I D I- 22.20 22.40 22.60 22.80 23.00 m/z 146.10 14.80% 96 165 i 29 39 51 63 74 83 l 115 126 139 152 j 176 [ I | । । । । । । f I T I 'i । "i | । । । । । I ’ I i I । > i' । । । r । r | । । r I । । । । । < । । । । i । > > । । । । i ( r'j । । । । |' I । i f“| r li TTi ill । i r 1t TT’T /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125848: Anthracene, 9-methyl- 192 - 22.20 22.40 22.60 22.80 23.00 5000 m/z 193.10 14.58%

96 27 39 51 63 82 ,|| 115 126 139 152 165 176 J ' r " ■ i1111 r TTTTTTTTTTT /I i ri'| rt i| 11 ri ffypem 11' 11111111111 iii 11111 111111|' T-p-r m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125849: Anthracene, 9-methyl- ................ 11* *‘I’*’ * ' | 1 ' 11 pr 192 22.20 22.40 22.60 22.80 23.00 m/ Z 96.20 13.48%

5000

96 165 28 39 51 63 74 83 l 105 115 126 139 152 | 176 | । । । i ।'1 । i । i i11 । । । । |1 k । < । । l h । । । . 1T1 I‘ i'I'i rl I i'| 1'1111 i111' r I I . |~I I I I r ’it ! | l rl 1 , | "‘I TTTT 1 I I 1 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00

10603.D 050102.M Thu May 09 09:06:51 2002 Page 9

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