GCMS analysis results for sample AE10609, May 10 2002

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Laboratory report detailing GC/MS analysis of sample AE10609 including surrogate recovery data in May 2002.

NYC-WTC_000045643–000045661

Folder label: “GCMS X 5/3/02 A 5/7/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050702\10609.D Vial : 12 Acq On 7 May 2002 10:06 pm Operator: Mclean Sample 5/3 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98. L Peak Number 8 Phenanthrene, 9-methyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 22.58 0.31 ug/L 352514 Phenanthranene-dl0 22.96 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 2 3-(2-Methoxy-5-methylphenyl)acry... 192 C11H1203 103986-76-1 50 3 Phenanthrene, 3-methyl- 192 C15H12 000832-71-340 4 Anthracene, 9-methyl-____________________ 192 C15H12 000779-0242 40 Abundance Scan 3319 (22.580 min): 10609. D (-3312) (-) m/z 192.10 100.00% 192

5000

। । । । > । । । । i i 11 । । । । । “I 1 ।' । । 92 96 146 160 22.20 22.40 22.60 22.80 23.00 42 ■ । ■ 11 ■ 1111111 * ।. 11111111111111 70 2, 118 I I I I I I I I I > I I I t I I I I I I I > I I 1' ।' " pangapas m/z 191.00 20.05% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192

5000 22.20 22.40 22.60 22.80 23.00 m/z 193.10 17.01% 96 165 29 39 51 63 74 83 J 115 126 139 152 11—01—00100010700100009 1111' I''1111 —l t i l 111 lllllllll " I" 176 I. I m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80954: 3-(2-Methoxy-5-methylphenyl)acrylic acid 161 192 1 I 1 1 1 1 I 1 ' ' 1 I ' 1 ' ' I ' 1 ' 1 I ' 22.20 22.40 22.60 22.80 23.00 5000 105 m/z 96.10 12.90% 77 132 | 91 115 , 145 39 51 65 ‘ I I . 175 Ll— 11 " " 11 " lrr ' lr 1 I r । rllr 111 ‘m rrilljr T । । । । । ill । । । । । ।' ■q-H-

mlz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81041: Phenanthrene, 3-methyl- __________ I I | [ _______ . . —i l [—i I i [ r 1 1 I । । । i —I ——— —kt — 192 22.20 22.40 22.60 22.80 23.00 m/z 146.10 12.12% 5000

96 EE 27 39 51 63 82 l 115 126 139 152 । 176 | m/z—> । p 1 1 1 । ' 1 1 । | । 1 < । | । ' 1 ' । I'l 1 1 | । r< i ['I 1 rl । । FIrgi 1 1 1 i'ii'i 1 । 1 r 1 1 । r 1 1 i‘| m 1 |‘l 1 1 1 । t'l t 1 [ 1 TTTI t i ’ Hr 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 1+ 1 11 22.20 22.40 22.60 22.80 23.00

10609.D 050102.M Thu May 09 09:14:12 2002 Page 11

NYC-WTC_000045658

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