GCMS sample AE12676 results, June 6 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C: \MSDCHEM\1\DATA\060402\12676.D Vial: 7 Acq On 4 Jun 2002 8:44 pm Operator: McLean Sample 6/4 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 11 Phenanthrene, 9-methyl- Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 22.53 0.26 ug/L 255132 Phenanthranene-dl0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 59 2 3-(2-Methoxy-5-methylphenyl)acry... 192 C11H1203 103986-76-1 53 3 Phenanthrene, 3-methyl- 192 C15H12 000832-71-3 45 4 Anthracene, 2-methyl- 192 C15H12 000613-12-7 45 Abundance Scan 3311 (22.533 min): 12676.D (-3302) (-) m/z 192.10 100.00% 192

5000 ........ I\......... m/z-> Abundance 0 ,1140.49 . 120 TDTTT 96 (Utt 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #81033: Phenanthrene, 9-methyl- „.a. | 146 160 । 22.20 22.40 22.60 22.80 m/z 191.10 17.16%

192 A 5000 ■ ■ i ‘ 1Tr 1II 22.20 22.40 22.60 22.80 m/z 193.10 15.71% 96 165 । । 29 39 51 63 74 83 a 115 126 139 152 j 176 , 0! I | I I I l rri 1 1-| 1 1 1 . |-, I I I | r’ii 1 | . rri rl’i rh r ■!■>>> pTI , 11 I I I | 1 ( ! l‘| I I. I ft I l , rt’t rI I rH | I l i’r n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80954:3-(2-Methoxy-5-methylphenyl)acrylic acid 192 161 n... d...... 22.20 22,40 22.60 22.80 "TT

5000 105 m/ z 96.00 14.14% 77 132 91 4 HlH— L 39 51 65 115 , 145 175 Of - —p Tgr miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81041: Phenanthrene, 3-methyl- 192 22.20 22.40 22.60 22.80 m/z 146.00 13.32%

5000'

96 E 27 39 51 63 82 1 115 126 139 152 । 176 2 0 ■ i ■ ■" i" " i" " i" " i " i ■r" r11 r|,i1111 rr 111 r"'1111"1111 rr ■ ■1 > fi 1 < 11 i'i'i 11 > । t-i 111 i’ Wtt m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80

12676.D 060302.M Wed Jun 05 14:04:45 2002 Page 14

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