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GCMS analysis results for sample AE11928, June 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11928 conducted on June 4, 2002.

NYC-WTC_000013496–000013523

Folder label: “GCMS X 5/22/02 A 5/23/02

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Scanned page image, NYC-WTC_000013515
OCR text

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\052302\11928.D Vial: 8 Acq On : 23 May 2002 3:40 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 12 Phenanthrene, 9-methyl- Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

22.54 0.28 ug/L 313082 Phenanthranene-dl0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 W 2 Anthracene, 9-methyl- 192 C15H12 000779-02-2 42 3 Anthracene, 2-methyl- 192 C15H12 000613-12-7 42* 4 9H-Fluorene, 9-ethylidene- 192 C15H12 007151-64-6 40 Abundance Scan 3312 (22.539 min): 11928.D (-3297) (-) m/z 192.10 100.00% 192

5000

I 1 1 ‘ ‘ F

40 70 82 96 146 160 22.20 22.40 22.60 22.80

m/z-> 0 118 TITT 111111111111111111111111111111111111111111111 2030405060 70 8090 100 110120 130140 150 160 170 180 190 200 mmmm Hpr m/z 191.00 19.74% Abundance #81033: Phenanthrene, 9-methyl- 192

5000 22.20 22.40 22.60 22.80 m/z 193.10 14.34% 29 39 51 63 74 83 *0 115 126 139 152 165 176 I 0: 110PIPTPTTTTTTNLTTTITTTTTTTTTTTTTTTTT “ I' ‘ niz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125849: Anthracene, 9-methyl-

■ ■ i ■ ■ ■ ■ । ■ 1***I***l 22.20 22.40 22.60 22.80 5000 m/z 146.10 14.13%

96 165

m/z-> 0 ■ I'' 28 39 51 63 74 83 | 105 115 126 139 152 ,| 176 „ ■ > rprri ' l'" " I t’ri rP t’ti r rrl r ■. । r ’t 11 ■ । ri ।. । r’1 । r th । > it 11 ■ rt 20 30 40 50 60 70 80 90 100 110120 130140 150160 170180190 200 4 Abundance #125844: Anthracene, 2-methyI- 22'20 2240 260 22.80 ' ' ‘ 192 m/ z 96.00 13.67% 5000

22 96 165

miz—> 0 TP3I01—0071m92——B3—3—gu 63 74 ' A3.il.. 115.... 4-rTTTT 2030405060 70 8090 100 110120 130140 150 160170 180 190 200 22.20 22.40 22.60 22.80

11928.D 052202.M Wed May 29 09:48:50 2002 Page 15

NYC-WTC_000013515

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NYC-WTC_000013515Source: NYC Law Department, mirrored locally

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