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GCMS analysis results, sample AE09151, May 2002

Machine-extracted title · confidence 100%

GCMS analytical report for environmental sample AE09151 including surrogate compound data from May 15, 2002.

NYC-WTC_000022795–000022811

Folder label: “GCMS X 5/8/02 A 5/10/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\050902\9151.D Vial: 18 Acq On : 10 May 2002 5:58 am Operator: Mclean Sample : 5/8 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 4 Phenanthrene, 9-methyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.36 ug/L 529623 Phenanthranene-dl 0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 59 2 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 42 3 Phenanthrene, l-methyl- 192 C15H12 000832-69-9 42 4 Anthracene, 2-methyl- 192 C15H12 000613-12-7 42 Abundance Scan 3318 (22.574 min): 9151. D (-3311) (-) m/z 192.10 100.00%| 192

5000

82 96 146 160 । R 22.20 22.40 22.60 22.80 23.00

m/z-> 42 54 0 TIWTTTTTHTHTHTTT — -‘11111 70 7 ,| 122 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 L m/z 191.10 16.29% Abundance #81033: Phenanthrene, 9-methyl- 192

5000 22.20 22.40 22.60 22.80 23.00 m/z 193.10 16.23%|

mlz-> 0 29 39 51 _ 63 74 83 96 I 165 115 126 139 152 , 176 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 TH ll. Abundance #125842: Phenanthrene, 2-methyl- 192

22.20 22.40 22.60 22.80 23.00 5000 m/z 96.10 14.65%

96 27 39 51 63 82 1 115 126 139 152 195 176 , 0 TPTmmua - +TTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTHTT mz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125856: Phenanthrene, 1-methyl- 192 22.20 22.40 22.60 22.80 23.00 m/z 146.10 13.77% 5000

96 P

m/z-> 27 39 51 0 ' i" " i" " i" " i'" ■ i 63 ■i 82 ,|| , 115 126 139 152 120 178 1 +TTTTTTTTTTTTTTTTTTTTTTTTTTHTTHTT TT 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 1 22.20 22.40 22.60 22.80 23.00

9151.D 050102.M Mon May 13 11:28:03 2002 Page 7

NYC-WTC_000022808

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NYC-WTC_000022808Source: NYC Law Department, mirrored locally

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