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GCMS analysis results for sample AE11418, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11418 conducted on May 30, 2002.

NYC-WTC_000025386–000025402

Folder label: “GCMS X 5/16/02 A 5/20/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\052002\11418.D Vial : 8 Acq On : 20 May 2002 6:59 pm Operator: Mclean Sample : 5/16 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 5 Phenanthrene, 9-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.27 ug/L 300571 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qua

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 50 2 2,5-Dihydrophosphole, 3-methyl-l... 192 C11H13OP 1000196-97-5 45 3 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5/45 4 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 42 Abundance Scan 3319 (22,580 min): 11418. D (-3311) (-) m/z 192.10 100.00% 192

5000

96 70 82 146 160 ...... ... A 22.20 22.40 22.60 22.80 23.00

mfe-> 0 PH , 118 | 1 I I 1 | , , , , | 1 1 411 1 | 1 1 > r| rHST 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ''' 1 ।, 111,, 11,, 111 — m/z 191.10 21.48% Abundance #81033: Phenanthrene, 9-methyl- 192

5000 117 22.20 22.40 22.60 22.80 23.00 m/z 96.10 16.01% 96 155 ।

m/z-> 29 39 51 01 TI’u—nuonTHmuuuumOuTTTT 63 74 83 l 115 126 139 152 I 176 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 , U Abundance #80965: 2,5-Dihydrophosphole, 3-methyl-1 -oxo-1 -phenyl- 164 192 .... 0... a. 22.20 22.40 22.60 22.80 23.00 5000 99 m/z 193.00 15.23% 115 47 77 177 67 ’ 125134 146 p 87,-HH 11155 27 38 |,57 , 0 TITTTTTTTT 1111 '11'' '11 HmH ‘n-rp-r miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80950:1,5-Naphthalenedithiole 192 22.20 22.40 22.60 22.80 23.00 m/z 146.10 14.87%

5000 115 128 159 40 57 69 79 96 147 177 ............ .......... ......................... 0- --------HH I । -HH THyur 1’111 m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00

11418.D 050102.M Thu May 23 10:46:09 2002 Page 8

NYC-WTC_000025398

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NYC-WTC_000025398Source: NYC Law Department, mirrored locally

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