GCMS analysis results for sample AE11418, May 2002

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Data File : C:\MSDCHEM\1\DATA\052002\11418.D Vial: 8 Acq On : 20 May 2002 6:59 pm Operator: Mclean Sample : 5/16 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 4 3-Pyrrolidinol Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

7.73 0.29 ug/L 227341 1,4-Dichlorobenzene-d4 9.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Pyrrolidinol 87 C4H9NO 040499-83 ' 37 2 2-Propanone, 1-cyclopropyl- 98 C6H10O 004160-75 25 3 Ethanone, 1-cyclobutyl- 98 C6H10O 003019-25 4 5-Hexen-2-one Abundance Scan 792 (7.733 min): 11418.D (-788) (-) 4 98 C6H10O m/ z 000109-49 43.10 10 3. 5000 MMWdvwym 58 87 98 7.40 7.60 7.80 8.00 I 51 miz-> 0- 5 --TT m " idr44 HH 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 HH+ 1’1 m/z 58.05 30.73% Abundance #4163: 3-Pyrrolidinol 43 MMMWApr/ "WMArwpwal 5000 7.40 7.60 7.80 8.00 57 68 87 m/z 87.10 17.14% [1 ‘ 11 ! 11111 , ++77.,824 0-111111111171110111111111013711 ’7711 r1" r ■ ■111711 miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #5149:2-Propanone, 1 -cyclopropyl- 43 ■ ■ i ■ ■ ■ ■ ।

wo 7.40 7.60 7.80 8.00 5000 m/z 44.10 14.57%

55 27 83 98 50 69 Of1 11 1 | 11 1 1 |11 ■ 11 1 " 11 1 I ' I | ‘ u 11 ri i I । 11 TOTTTPTTTTTTTTT TTTTTTTTTTTTTT m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #5002: Ethanone, 1 -cyclobutyl- ' ■ । ■ 1 ■ r 43 55 7.40 7.60 7.80 8.00 m/z 83.00 12.24%

5000 27 83

m/z-> 0 +++'I""!"1' —PhmPTT 98

5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 p 1 1 111 1111’[ 11 1114/1/+4I 7.40 7.60 7.80 8.00

11418.D 050102.M Thu May 23 10:46:07 2002 Page 7

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