GCMS analysis results for sample AE11417, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\052002\11417.D Vial: 7 Acq On : 20 May 2002 6:10 pm Operator: Mclean Sample : 5/16 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 4 3-Pyrrolidinol Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 7.73 0.30 ug/L 247293 1,4-Dichlorobenzene-d4 9.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pyrrolidinol 87 C4H9NO 040499-83-0 9 2 4-Penten-2-one, 4-methyl- 98 C6H10O 003744-02-3 9 3 2 -Propanone, 1-eye1opropyl- 98 C6H10O 004160-75-2 9 4 Ethanol, 2-(pentyloxy)-, acetate 174 C9H18O3 005312-09-4 9 Abundance Scan 792 (7.733 min): 11417. D (-780) (-) m/ z 43.10 100.00% 4)3

5000 M 58 87 39 48 83 98 7.40 7.60 7.80 8.00 ........... ,|J| 0 [ ‘ ‘ 1 I 1 ' 1 1 I ‘ ' 1 "TT ■ I f' rhitHti । ■ ■ > ■ । ■ 1111 I.1 .... I.......... I I I I I I I I I I I I I I I m/ Z 58.10 25.47%

VBw m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #4163:3-Pyrrolidinol 43

MMWWWnywMut 5000 7.40 7.60 7.80 8.00 57 87 m/ Z 87.10 19.77% 68

m/z-> 0 47 52 I " '111111 +4—l72,77..83 1111. ।.. >. ।... ■ ।. 11.. 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #110033: 4-Penten-2-one, 4-methyl- 43 --

7.40 7.60 7.80 8.00 5000 m/z 55.10 12.40% 83 39 55 98

mfe-> Ot 4 -H- 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 -

Abundance #5149: 2-Propanone, 1-cyclopropyl- 43 7.40 7.60 7.80 8.00 m/z 41.10 12.02% 5000

55 27 39 83 98

m/z~> 0 mHH +H 4 50 69 > J I J I | I I I I | I I I I | Tt p I ! I | > mmmmm "11 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 7.40 7.60 7.80 8.00 ____

11417.D 050102.M Thu May 23 10:45:21 2002 Page 7

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