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GCMS analysis results for sample AE11423, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11423 conducted on May 30, 2002.

NYC-WTC_000025479–000025493

Folder label: “GCMS X 5/16/02 A 5/20/02

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Scanned page image, NYC-WTC_000025490
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052002\11423.D Vial: 13 Acq On : 20 May 2002 11:03 pm Operator: Mclean Sample : 5/16 eh Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 4 3-Pyrrolidinol Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 7.73 0.27 ug/L 206384 1,4-Dichlorobenzene-d4 9.93 Hit# of 5 Tentative ID MW MolForm CAS# Qua

1 3-Pyrrolidinol 87 C4H9NO 040499-83-0 9 2 Ethanone, 1-cyclobutyl- 98 C6H10O 003019-25-8/7 3 2-Propanone, 1-cyclopropyl- 98 C6H10O 004160-75-2 7 4 4-Penten-2-one, 4-methyl- 98 C6H10O 003744-02-3 7 Abundance Scan 792 (7.733 min): 11423. D (-786) (-) m/z 43.10 100.00%

LL 43

5000 wyNMWWWAN 58 87 1 1 । ■ 1110 98 7.40 7.60 7.80 8.00

m/z-> Ormpmmmpmmmmmmmm —1— .... | i1"' p'111 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 m/ z 87.00 24.18% Abundance #4163: 3-Pyrrolidinol 43

5000 1 ' i ' ' 1 ' i ' ‘ 1 1 1 1 1 1 1 I 7.40 7.60 7.80 8.00 57 68 87 m/ z 58.05 23.41%

miz- > 0b p' " r ‘" i " " i " " r1" p " ‘ i +45R4441 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 .111111,771/821/1 r "1 p " 'P1" r " Abundance #5002: Ethanone, 1 -cyclobutyl- 43 55 N" 7.40 7.60 7.80 8.00 5000 m/ z 83.00 13.68% 27 83

mfe-> ot 111 15 । p " 1111111 +1 1 ■ ■ I I .. , . ). 1 t 1 | 1 ! 1 I | > 1 1 ! | 1 ! 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 popngaga 98

Abundance #5149: 2-Propanone, 1-cyclopropyl- ' ■ i 1 ■ ■ 1 i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ' ■ ' i 43 7.40 7,60 7.80 8.00 m/z 98.20 10.43% 5000

55 27 50 69 83 98 0b TTTH TOhTTTTRTTTTTTTT-HTmTTTT 1 1 I 1 1 1 1 I m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 7.40 7.60 7.80 8.00

11423.D 050102.M Thu May 23 10:49:43 2002 Page 7

NYC-WTC_000025490

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NYC-WTC_000025490Source: NYC Law Department, mirrored locally

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