GC/MS results for unknown compounds and surrogates, sample AE10985, May

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\051402\10985.D Vial: 14 Acq On : 15 May 2002 12:06 am Operator: Mclean Sample : 5/10 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 7 3-Pyrrolidinol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

7.72 0.50 ug/L 395378 1,4-Dichlorobenzene-d4 9.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pyrrolidinol 87 C4H9NO 040499-83-0 32 2 2-Propanone, 1-(1-methylethoxy)- 116 C6H12O2 042781-12-416 3 Acetone 58 C3H60 000067-64-/ 9 4 Furan, 2,3-dihydro-2,5-dimethyl- 98 C6H10O 017108-52/0 9 Abundance Scan 790 (7.721 min): 10985.D (-785) (-) m/ z 43.10 0.00% 43

5000 58 87 98 7.40 7.60 7.80 8.00 O+ .................... I] + 49,1 1 1 Tmnn । । i i । j i i i । 169 < lT' 1 1 I 1 ‘ 1 1 | ■ I ' ■ ' ■ I X TTT J.............. m/z 58.10 23.10% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance

5000 43 #4163: 3-Pyrrolidinol

w-MWWANWW WPMVWAWW ' 1 ' I ‘ 7.40 L ‘ I ' ' 1 ' I ‘ 7.60 7.80 ‘ ' I ' ' ' ‘ 1 8.00 57 68 87 m/z 87.10 19.02% 01 11 174*41 * *’1*1’I 50 +5141111477 60 70 80 90 t 11' । j . . . । 100 । i < । . . . . ( 110 120 . miz-> 10 20 30 40 Abundance #4364:2-Propanone, 1 -(1 -methylethoxy)- 43 . MM ' ' I ' 1 ' ' I 7.40 7.60 7.80 8.00 5000 m/Z 57.10 14.44% A 27 58 73 n/z-> 01 -14+3744 10 20 30 40 i ■ • i ■ 50 ill I 83 101 1 i ■ ■ ■ ■ । ■ 1 1 ■ i ■ ' ■ ■ । ' 1 ' ■ । ' ' 60 70 80 90 100 110 115 ' ■ 1 ■ । ■ ■ 120 Abundance #5734: Acetone ‘ I 43 7.40 7.60 7.80 8.00 m/z 41.10 13.64%

5000 15 58

27 0 ■ • ■ । । I * ■ i ■ lli, . . rl । " i " i t ■ ■ ■ ■ । ■ i ■ ■ ■ ■ i ■ ■ ■ ■ । । । - ■ ■ ■ । ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120

10985.D 050102.M Thu May 16 14:42:38 2002 Page 10

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