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GCMS analysis results, sample AE09332, May 2002

Machine-extracted title · confidence 100%

GCMS analytical report for environmental sample AE09332 including surrogate compound data from May 15, 2002.

NYC-WTC_000022886–000022901

Folder label: “GCMS X 5/8/02 A 5/10/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\050902\9332.D Vial: 22 Acq On : 10 May 2002 9:13 am Operator: Mclean Sample : 5/8 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Phenanthrene, 9-methyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.32 ug/L 439453 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual^

I Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 50 2 2,5-Dihydrophosphole, 3-methyl-l... 192 C11H130P 1000196-97-5 45 3 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 5 4 Anthracene, 9-methyl-____________________ 192 C15H12 000779-02-2 40 Abundance Scan 3319 (22.580 min): 9332. D (-3312) (-) m/z 192.10 100.00%| 192

5000

96 146 160 .. R. A, /z-> 42 54 70 82 120 0 TTTTTTTHTT 'I............ I1"1! 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 -H+ Ip 22.20 22.40 22.60 22.80 23.00 m/z 191.10 20.52%! Abundance #81033: Phenanthrene, 9-methyl- 192

5000 n. 22.20 22.40 22.60 22.80 23.00 rn/z 146.10 14.63% 96 165 i । 29 39 51 63 74 83 1 115 126 139 152 | 176 O+ ' I " 1 ‘ I " "'I " " T" " I ' 11 ' I'1' rf H 1'' I " ■' I'-'111'1 ■111''-'I " 1 ■ I'1" rp1!1.. ।. r4t ।.. rHt " i'1 mz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80965: 2,5-Dihydrophosphole, 3-methyl-1-oxo-1 -phenyl- 192 164 0/ 22.20 22.40 22.60 22.80 23.00 5000 99 m/z 193.10 13.74%| 115 47 77 177 67 125 146

m/z-> 0 —2738. 157L +7+ H .. . '"I'"'I i ""I1 " i" 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80950:1,5-Naphthalenedithiole 192 22.20 22.40 22.60 22.80 23.00 m/z 96.10 12.52%|

5000 115 128 159 40 57 69 79 96 147 177 0 ----- r t1 A. 1 TTIur ■ ■ i" /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00

9332.D 050102.M Mon May 13 11:43:44 2002 Page 8

NYC-WTC_000022898

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NYC-WTC_000022898Source: NYC Law Department, mirrored locally

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