GCMS analysis results, sample AE09154, May 2002

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GCMS analytical report for environmental sample AE09154 including surrogate compound data from May 15, 2002.

NYC-WTC_000022819–000022849

Folder label: “GCMS X 5/8/02 A 5/10/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\050902\9154.D Vial: 19 Acq On : 10 May 2002 6:47 am Operator: Mclean Sample : 5/8 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 Phenanthrene, 9-methyl- Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.30 ug/L 336142 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 42 2 2-Imidazolidinone, 1-methoxy-3-p... 192 C10H12N2O2 052420-43-6 38 3 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 38 4 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 36 Abundance Scan 3319 (22.580 min): 9154.D (-3310) (-) m/z 192.10 100.00% 192

5000

— 96 146 160 42 52 70 82 22.20 22.40 22.60 22.80 23.00 118 |, 207 0 mTHpTTHTTTTTT TJUTTTTTTTTTTT TTTT m/ Z 191.10 18.92% n/z-> 20 30 40 50 60 70 80 90 100110120130140 150160 170180190 200 210 Abundance #81033: Phenanthrene, 9-methyl- 192

5000 22.20 22.40 22.60 22.80 23.00 m/z 146.10 17.73% 96 165 i । 01 63 74 83 115 126 139 152 | 176 29 39 51 TTTTTTTTTTTTTTTTTTTTTTTTTTTWTTTTTTTHTTT " r " ' i" n/z-> :20 30 40 50 60 70 80 90 100110120130140150160 170180190 200 210 Abundance #80907: 2-Imidazolidinone, 1-methoxy-3-phenyl- 106 192 11. —A ' I ' ' ' ' 1 1 22.20 22.40 22.60 22.80 23.00 77 119 162 5000 rn/z 96.10 16.05% 42 56 91 28 134

ti/z-> 0 HHITHT 11'" ■ ■" !■ I" I ■ "■ I ■ 20 30 40 50 60 70 80 90 100110120130140150160 170180190 200 210 " i'"11" " i I'''' I

Abundance #81030:4-Hydroxy-3,5-dimethylcinnamic acid 1 I 1 ' ' 1 I ' ■ ' i ■ ' 1 1 i ' 192 22.20 22.40 22.60 22.80 23.00 m/z 193.10 14.21%

5000

89 175 63 145 45 135 |, I, , 77 , i ' 105; i7 163

n/z—> 0 -4 I, +tttH"prr । i’ttert 1111 ’t’i 111 "’r]’ 111 [ ri 111 ri1!) 111 ii i1 20 30 40 50 60 70 80 90 100110120130140150160 170180190 200 210 H 22.20 22.40 22.60 22.80 23.00

9154.D 050102.M Mon May 13 11:28:51 2002 Page 9

NYC-WTC_000022832

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