GCMS analysis results, sample AE09154, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\050902\9154.D Vial: 19 Acq On : 10 May 2002 6:47 am Operator: Me lean Sample : 5/8 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 5 4-Penten-2-one, 4-methyl- Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

7.73 0.33 ug/L 273595 1,4-Dichlorobenzene-d4 9.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4-Penten-2-one, 4-methyl- 98 C6H10O 003744-02-3 2 1-Pentanamine 87 C5H13N 000110-58-7 12 3 Octanoic acid, 7-oxo-, methyl ester 172 C9H16O3 016493-42-8 12 4 Ethanol, 2-(pentyloxy)-, acetate 174 C9H18O3 005312- -4 10 Abundance Scan 791 (7.726 min): 9154.D (-786) (-) m/ z 43.10 100.00% 43 __

5000 AMWWPyww 58 87 98 7.40 7.60 7.80 8.00 207 0 ‘ i * ■ ■' i ' i"'' i11'11' ■111" " i" ■ ■ i ■"11"1' i' ‘'11" " i ■'1 ■ i" ■ m/z 58.10 29.96% n/z—> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #110033: 4-Penten-2-one, 4-methyl- 43

MMAr"MW 5000 ■ 1 ' i ■ ■ ‘ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ 1 ' ' i 7.40 7.60 7.80 8.00 83 m/z 87.00 22.14% 55 98 ■ t■• •■। ■■■ ■। ■ 11 । । i'■■*i*■" ।■■•■।।■i■■* * ।। • ■' ■ । * 0 "T niz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #108255:1-Pentanamine 33 1 ' ■ i ■ ■ ■ ■ । ■ r ■ ■ ■ ■ i1 1 ' ■ i 7.40 7.60 7.80 8.00 5000 m/z 41.10 16.47%

01- 18 41 55 70 87 n/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #110110: Octanoic acid, 7-oxo-, methyl ester 43 7.40 7.60 7.80 8.00 m/z 55.10 16.29%

5000 87 59 69 130 98 115 141 _

n/z-> 0 ’ ’0 HHH I ——0—00110000000001 172 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 7.40 7.60 7.80 8.00

9154.D 050102.M Mon May 13 11:28:50 2002 Page 8

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