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GCMS analysis results, sample AE09973, May 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE09973 showing surrogate recovery and unknown compounds from May 9, 2002.

NYC-WTC_000044025–000044054

Folder label: “GCMS X 4/25/02 A 5/7/02”

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NYC 9/11 Public Portal Document

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Data File C:\MSDCHEM\1\DATA\050602\9973.D Vial : 21 Acq On 7 May 2002 3:59 am Operator: Mclean Sample 4/25 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 9 3-Penten-2-one, 4-methyl- Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T. 5.02 0.33 ug/L 234301 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Penten-2-one, 4-methyl- 98 C6H10O 000141-79-7 43 2 2-Pentene, 3,4-dimethyl-, (E) - 98 C7H14 004914-92-5/43 3 2-Pentene, 2,4-dimethyl- 98 C7H14 000625-65-0 38 4 3-Hexen-2-one 98 C6H10O 000763-93-9 38 Abundance Scan 331 (5.024 min): 9973. D (-324) (-) m/z 83.10 LOO.00% 83 55

40 5000 49 98 I I I I I I I r I I I I I 11177111 l

4.60 4.80 500 5.20 5.40 88 n/z-> 1] I _ I ~ l " I

10 20 I I ( > I

30 I I I

40 l 5060 1

70 I

80 I I I I I I ■ I f I I )

90 100 m/z 55.10 77.05% Abundance #116425: 3-Penten-2-one, 4-methyl- 55 83

5000 ...... MAM .. .................... 43 [ ' 1 1 *1 11 1 I I 1 1 1 I I I I I I I ■ ■ I 98 4.60 4.80 5.00 5.20 5.40 29 m/z 40.10 51.64% w~vNWWMWM( 38 . 50 | , 62 67 । । । iiii । > । i* I । । -1 —————— 77 1—4rt 1-89,, I ' 1 n/z-> 10 20 30 40 50 60 70 80 90 100 Abundance #32908: 2-Pentene, 3,4-dimethyl-, (E)- 55 83 i ■ ‘ ' i ' 1 1 ' i 1 ' 1 ■ i ■ ■ 1 1 i ■ 1 '

41 4.60 4.80 5.00 5.20 5.40 5000 m/z 39.20 30.34% 27 98 4 15 69 I 1 ' 1 ' 1 1 +30 .36, — J, . 50, 1 I. 63 | |, 77 , —91 i 1 1 Tl/Z“>

Abundance 10 20 50 60 70 80 90 100 40 #32912: 2-Pentene, 2,4-dimethyl- 83 p-T- 4.60 4.80 5.00 |L_LA 5.20 5.40 55 m/ z 98.10 29.87% 5000- 41 4 27 98 15 50 । | 62 j7 77 ...... 1...... 1132 I I | - I I I I | I I I I j I : , I • I I I ‘ 1111111 I I I ‘ I ■ 111 —91 1 1 । 1 1 1 ■ । 1 ' m/z-> 10 20 30 40 50 60 70 80 90 100 4.60 4.80 5.00 5.20 5.40

9973.D 050102.M Tue May 07 15:52:00 2002 Page 13

NYC-WTC_000044042

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GCMS analysis results, sample AE09968, May 2002 · Box DEP Box 25

NYC-WTC_000043938

Gas chromatography-mass spectrometry analysis report for sample AE09968, detecting unknown compounds and 2,4-DDD surrogate with 78% recovery, dated May 9, 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996

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