GCMS sample analysis results for AE10603, May 10 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050702\10603 .D Vial : 8 Acq On 7 May 2002 6:50 pm Operator: Mclean Sample 5/3 kb Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 2 3-Penten-2-one, 4-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

5.02 0.27 ug/L 266809 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Penten-2-one, 4-methyl- 98 C6H10O 000141-79-7 2 3-Hexen-2-one 98 C6H10O 000763-93-91 3 3-Penten-2-one, 4-methyl- 98 C6H10O 000141-79-7, 4 2-Pentene, 3,4-dimethyl-, (Z)- 98 C7H14 004914-91-4 Abundance Scan 329 (5.012 min): 10603.D (-324) (-) m/z 83.10 100 00% 55 83

5000 43 98 ____________________ AAA____________ A । i । i i । I । i i f l | | 1 I I | T I

3& 50 4.60 4.80 5.00 5.20 5.40 ' i1' " i'11' r 111 r lid । ! . ! | I I I ! p I > I p I ! ! | I ! I . | I I 1111 " I' TTPTTTT ‘I’T m/ z 55.10 92.04% m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #116425: 3-Penten-2-one, 4-methyl- 55 83

5000 43 1 1 1 1 1 Tit 11 ' 98 4.60 4.80 5.00 5.20 5.40 29 m/ Z 43.10 47.60%

/z-> Abundance 38 50 | . 62 67 MIHlipe...... lllllllrpn.il ill TTTTTt 77 , 89 17 ‘Tir I I I I 1 I I I 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 #116424. 3-Hexen-2-one 83 1111111"

ra/AMWWV W I 1 1 1 ' 4 1 * ’ 1 | 1 1 1 1 | » । 1 i | i » 55 4.60 4.80 5.00 5.20 5.40 5000 43 m/z 98.00 38.24% 98 29 I I I I I I I I 23I I J,| I I 1 I I I I 38 1 ■i । । 50 mllir , । | I । I i ,111 11 163 69 77 11111111 [ 111 11 I 1111 11 i 93 I I I I I I I I I ■ > I t r I......... /z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #116450: 3-Penten-2-one, 4-methyl- 55 83 4.60 4.80 5.00 5.20 5.40 m/z 39.10 34.04% 98 43 5000 28

50 । , miz-s ' r' " i'1" i1 3& I 67 r llipl|l|ll I P 11 I [ 1111 TTI—ETTETT21111117 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 I | । ! I I | I I > I | I I TTTT LA I ‘M t-|-i . . A)AAM . , TII । , । i' । 4.60 4.80 5.00 5.20 5.40

10603.D 050102.M Thu May 09 09:06:43 2002 Page 5

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