GCMS sample analysis results for AE10603, May 10 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050702\10603.D Vial: 8 Acq On 7 May 2002 6:50 pm Operator: Mclean Sample 5/3 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 1 Toluene Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 4.33 0.28 ug/L 270055 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Toluene 92 C7H8 000108-88-3/86 2 Toluene 92 C7H8 000108-88-3 86 3 Toluene 92 C7H8 000108-88-3 86 4 Cyclobutene, 2-propenylidene- 92 C7H8 052097-85-5 72 Abundance Scan 213 (4.331 min): 10603.D (-207) (-) m/ z 91.10 100.00% 91

5000 ...................... . I I , I I I "I I I 1 > I I I ' I " ) I I I I I I 39 _ 65 4.00 4.20 4.40 4.60 35 I. 45 51 58 , | i i | i i I i | * । i I | i i > I । I I i i । i । i i-|~ r rl । 86 , i r i i । i i i i | i i । । । । i i i । I i ' f 'i ■ 11111 > ■ 111 m/z 92.10 59.72% r' ।1 r 1111 m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #117292: Toluene 91

5000 —। "I > - «> | 1 ... p I I 1 I | ! I I I ] 4.00 4.20 4.40 4.60 m/ z 39.10 13.19% 39 F4 65 27 .1 45 , 55 61| | 73 77 86 ,, I'11 ■ i TTT | I I I trprtt ri t [ I I I I | I I I I | I I I I | J । i i [ i i । | j I 1 I I [ I I I I | I I I I | HP m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #37326: Toluene 91 I .MM# 4.00 4.20 4.40 4.60 4 5000 m/z 65.10 12.07%

27 31 39 45 51 57 61,65 73 .............. 77 86 PTrpu’l i i । i I ri ] i i i i [-ft t-|'| bi | i | I । । । | I I i । । । । n tl I f | H । i । । । i ।i । । । i rr। i i । | | TTTI m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #117283: Toluene 91 4.00 4.20 4.40 4.60 m/z 93.10 7.01% 5000 39 65 27 45 51 23 । 31 35 । " 111111111"1111 11111 61, 1 73 77 81 86 ,, I I I I I l+f jl'l I I 11 I I I [ I f I I I I I I I I I I I I I • ' | 1 1 * ‘ | "I1 । 1 'i | i 'i । I [ i i i i |

n/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 4.00 4.20 4.40 4.60

10603.D 050102.M Thu May 09 09:06:40 2002 Page 4

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