GCMS blank analysis results for VOCs, May 9 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050702\0503LB.D Vial : 5 Acq On 7 May 2002 4:24 pm Operator: Mclean Sample 5/3 kb Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 1 Toluene Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

4.35 0.25 ug/L 228283 1,4-Dichlorobenzene-d4 9.94 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Toluene 92 C7H8 000108-88-3 83 2 Toluene 92 C7H8 000108-88-3 83 3 Toluene 92 C7H8 000108-8843 80 4 Toluene 92 C7H8 000108-88-3 80 Abundance Scan 216 (4.348 min): 0503LB.D (-209) (-) m/ z 91.10 100. O 91

5000

39 65 ..... s....... I

4.00 I l l I-1

4.20 I I I I '" I “ I

4.40 I I I-1

4.60 | I I I-1 I

| 45 51 58 . | 86 ............. . ......... .।. ..... 'I 1 1 I 1 m/z 92.10 62.90% m/z-> 0 10 20 30 40 50 60 70 80 90 100 Abundance #117282: Toluene 91

5000 ...... I.......... 4.00 4.20 4.40 4.60 m/ z 65.10 12.87% 39 E 51 65 m/z-> 0 ........... 10 20 ..27..... 30 ,140,41 50fl1,...,.,60 U..,.. 70 780,. ^..90,11 1 ' I 1 100 Abundance #117292: Toluene 91 1 1 i ■ 1 1 1 i 1 ■ 1 1 i ' 1 1 ■ i ■ 1 ■ ■ i ' 4.00 4.20 4.40 4.60 5000 m/z 39.10 10.81%

39 M 65 27i .1 |' t 45 ■ | 1 ‘ 57 ,|.| 77■ 86,.

1....... |' i i_ । |_ J- । । । । । । i i । । । । I ।' 1 । t। '1 r 'I I I । । । । i । । । i-1 i I 1 ' i 1 m/z-> 0 10 20 30 40 50 60 70 80 90 100 Abundance #117281: Toluene 91 4.00 4.20 4.40 4.60 m/z 63.00 7.00% A 5000 39 65 P 51 1 — ——15 ————27—— 45,.1,,56,411, 77 86 , 1............... 1 i 1 1 1'' i 1 1 1 1 1 I I I I I I I I I 1 i 1 ■ 1 1 i 1 1 1 ' i ' m/z-> 0 10 20 30 40 50 60 70 80 90 100 4.00 4.20 4.40 4.60

0503LB.D 050102.M Thu May 09 09:20:57 2002 Page 4

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