GCMS sample analysis results, AE11901, June 4, 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\052202\11901.D Vial: 8 Acq On : 22 May 2002 7:31 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator:) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 8 Toluene Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 4.27 2.08 ug/L 1398360 1,4-Dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Toluene 92 C7H8 000108-88-3 86 2 Toluene 92 C7H8 000108-88-3 86 3 Toluene 92 C7H8 000108-88-3 80 4 Toluene 92 C7H8 000108-88-3 72 Abundance Scan 203 (4.272 min): 11901.D (-198) (-) m/z 91.10 100.00% 91

5000

* 39 50 65 84 4.00 4.20 4.40 4.60 0- .......................................... ..................................................... *441 m/z 92.10 58.83% ■nlz-> 0 10 2030405060 70 80। 90 100 Abundance #117283: Toluene 91

5000 —IIIIIIITT 4.00 4.20 4.40 4.60 39 m/z 65.10 13.06% 65 45 51 0- T Bid 22,27933.4444—44— 69,1,1, 70-77.864 I

iz-> 0 10 20 30 40 50 60 70 80 90 100 Abundance #117292: Toluene 91 ■ • i ' ■ • ■ i ■ ■ • ■ i ■ ‘ ■ ■ i ■ ' 4.00 4.20 4.40 4.60 5000 m/z 39.10 9.63%

54? 57 , 65| 39

m/z-> 0- ‘ ‘ I ' ‘ ' 1 I ‘ ‘ 0 10 ' I ‘ ' 20 27—44 45 11 30 40 III: ■ i 50 60 70i 1 77 86, i i 1 "''I'1 80 90 100 Abundance #117281: Toluene 91 4.00 4.20 4.40 4.60 m/z 63.10 8.31%

5000

39 E 51 65 . 0 1 15 27 ■ ■ I1 ' ' ' i • ■ ‘ ■ i • 11, I 1 . 177.1156, 11,1 , , TIT 77 86, i 100 1 •n/z-> 0 10 20 30 40 50 60 70 80 90 4.00 4.20 4.40 4.60

11901.D 052202.M Tue May 28 12:05:41 2002 Page 11

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