GCMS analysis results for sample AE11932, June 2002

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Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052302\11932.D Vial: 12 Acq On : 23 May 2002 6:56 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 8 Toluene Concentration Rank 4 R.T. ' EstConc Area Relative to ISTD R.T.

4.27 1.20 ug/L 818365 1,4-Dichlorobenzene-d4 9.90

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Toluene 92 C7H8 000108-88-3 47 2 1,5-Heptadien-3-yne 92 C7H8 003511-27-1 47 3 Toluene 92 C7H8 000108-88-3 38 4 Toluene 92 C7H8 000108/88-3 9 Abundance Scan 202 (4.266 min): 11932.D (-197) (-) m/ z 91.10/ 100. 91

5000 1 ■ i ■ ■ ■ ■ i W —— —

iz-> 0- 1* 0 10 20 30 38 40 tL1 50 52 60 63 70 79 . 80 90 98 — 100 m/z 4.00 92.00 4.20 4.40 4.60 58.59% Abundance #117281: Toluene 91

5000' ' ■ ■ ■ i ' ■ ■ ■ i 1 ■ ■1 i ■ ' ■ • i ■ ■ ■ 1 4.00 4.20 4.40 4.60 39 RR m/z 38.10 16.97% 27 E 51 65 miz-> 0- 1 * ‘ i■ ■ > ‘ , i < 0 10 15 — ■ i > 20 30 ,1147.1,571. 40 50 60 70 77 85 । 80 90 I ‘ • r‘ I 1 I

100 Abundance #117290:1,5-Heptadien-3-yne 91 ‘ ■ i ■ ■

4.00 4.20 4.40 4.60 5000 m/z 79.10 15.15% 51 39 65

0- 18 26 32 ii, ,45 1*1*11* 1 ~i1 ■11 r> ■ '‘I'l1 ,158. 1,7117785.1 ————— miz—> 0 10 20 30 40 50 60 70 80 90 100 Abundance #117283: Toluene ■ ■ i ‘ ■ * 1 I 14 91 4.00 4.20 4.40 4.60 m/z :39.10 14.81% 5000 A 1 39 ci 65 27 45 51 , . vl i 33,4144-57,4— 77 85 1 1_________ _ 0 ‘ ■ • i ■ ‘ Itit "I i 1 ■ 1 m/z—> 0 10 20 30 40 50 60 70 80 90 100 4.00 4.20 4.40 4.60

11932.D 052202.M Wed May 29 09:51:36 2002 Page 11

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