GCMS analysis results, sample AE09151, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\050902\9151.D Vial: 18 Acq On : 10 May 2002 5:58 am Operator: Mclean Sample : 5/8 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 3 4-Penten-2-one, 4-methyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

7.73 0.28 ug/L 288171 1,4-Dichlorobenzene-d4 9.94 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-Penten-2-one, 4-methyl- 98 C6H10O 003744-02-3 14 2 2-Propanone, 1-cyclopropyl- 98 C6H10O 004160-75-2 9 3 4-Methyl-2-pentyl acetate 144 C8H1602 00010 8-84-9 9 4 2-Pentanol, acetate 130 C7H14O2 00062 6-38-0 9 Abundance Scan 791 (7.727 min): 9151 .D (-785) (-) m/z 43410 100.00% 43

5000 58

miz-> 0- ............... I T-p-TT-r-p-T-r-ry-T-r-r-r-p- 10 20 30 40 —ll— .... I 87 98 50 60 * । >1 11 ।11- T" 70 80 90 100 110 120 130 140 150 7.40 m/ z 7.60 7.80 58.05 8.00 24.89%

Abundance #110033: 4-Penten-2-one, 4-methyl- 43

wWMw 5000 ■ ■ i ■ ■ ■ ■ i ■ ■ ' ■ i 1 ■ ■ ■ i 1 ■ ■ ■ । 7.40 7.60 7.80 8.00 83 m/z 87.10 17.01% 28 55 98

n/z-> 0- ...... ,1.1. 10 20 30 40 - 50 60 70 80 90 100 110 L Tr 120 130 140 150 Abundance #5149:2-Propanone, 1-cyclopropyl- 43 7.40 7.60 7.80 8.00 5000 rn/z 55.10 12.55% 55 27 83 98 69 0- .... PH 11' rp ■ I i ■1 ■ ■ i '' '' i1 ■ ■ ■ i' -pmmmpmt mfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #6126:4-Methyl-2-pentyl acetate 43 7.40 7.60 7.80 8.00 m/z 83.00 10.60%

5000 69 A 87

15 27 0 pipi ilip 1111 1 ' 1 . 1 .53.61. । | ' ....! | I , 11 I**’102 । 129 IIt-I****I*’***/ ■ 1 144 TTT m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 7.40 7.60 7.80 8.00

9151.D 050102.M Mon May 13 11:28:02 2002 Page 6

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