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GCMS blank analysis results for sample AE11379, May 21, 2002

Machine-extracted title · confidence 95%

Laboratory report showing GCMS blank analysis for sample AE11379 conducted on May 21, 2002, with results below minimum reporting levels.

NYC-WTC_000025054–000025071

Folder label: “GCMS X 5/15/02 A 5/17/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\051702\0515LB.D Vial : 16 Acq On : 18 May 2002 1:49 am Operator: Mclean Sample : 5/15 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 2 4-Penten-2-one, 4-methyl- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

7.73 0.36 ug/L 385827 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l 4-Penten-2-one, 4-methyl- 98 C6H10O 003744-02-3 9 2 Methyl 1-methylcyclopropyl ketone 98 C6H10O 001567-75-5 9 3 2-Propanone, 1-eye1opropy1- 98 C6H10O 004160-75/2 9 4 5-Hexen-2-one 98 C6H10O 000109-49-9 9 Abundance Scan 791 (7.727 min): 0515LB.D (-787) (-) m/z 43.10 TOO.00% 43 __

5000-

58 87 ' 1 ‘ 1 1 1 1 1 1 1 1 ' ' I 1t 1 ' 1 1 ' 1 ‘ I 98

mlz-> 0+ -HHRH .................... I + 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 69 ! TPTTT m/z 7.40 7.60 87.10 7.80 8.00 26.19% Abundance #110033: 4-Penten-2-one, 4-methyl- 43

5000 ' 1 i 1 1 ■, W............ 7.40 7.60 7.80 8.00 28 83 m/ Z 58.10 24.20% 55 98

m/z-> 0 lal,L.34 HHH soo 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #5005: Methyl 1-methylcyclopropyl ketone 43 WWWyuAw ' 1 1 1 1 ' 1 ' 1 1 1 ' 1 I ' 1 1 1 1 1 ' 1 ' 1 7.40 7.60 7.80 8.00 5000 m/ z 59.10 14.58% 55 29 83 98 I"1......... .................................... ... 50 , 63 69 77 | || 0 111, । r । h 1111, ■ i ■"11'11111"11" " r'1 ‘ r "' i11" r11' I"11 r "1 mfe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #5149: 2-Propanone, 1-cyclopropyl- 43 1 ' 1 I 1 ' ■ 1 । 1 7.40 7.60 .1.4.... 7.80 8.00 m/ z 41.10 13.97%

5000

55 27 0 I" " 11 ’" I TH - i1 ■ ■ ■ i"69 83 1 50 98 111" " i ■'" i1 ■111" " i'1" r111 r "1 r mfe~> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 7.40 7.60 7.80 8.00

0515LB.D 050102.M Tue May 21 11:58:09 2002 Page 5

NYC-WTC_000025062

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NYC-WTC_000025062Source: NYC Law Department, mirrored locally

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