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GCMS analysis results, sample AE09973, May 2002

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Laboratory report for sample AE09973 showing surrogate recovery and unknown compounds from May 9, 2002.

NYC-WTC_000044025–000044054

Folder label: “GCMS X 4/25/02 A 5/7/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050602\9973.D Vial: 21 Acq On 7 May 2002 3:59 am Operator: Mclean Sample 4/25 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 14 Phenanthrene, 9-methyl- Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T.

22.58 0.34 ug/L 339201 Phenanthranene-dl0 22.96 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 2 2,5-Dihydrophosphole, 3-methyl-1... 192 C11H130P 1000196-97-5 4 3 Anthracene, 9-methyl- 192 C15H12 000779-02-2 42 4 Anthracene, 2-methyl-_______________ 192 C15H12 000613-12-7/42 Abundance Scan 3319 (22.580 min): 9973.D (-3311) (-) m/z 192.10 100/00% 192

5000

. 40I 51 — 82i 96 146 160 A II 22.20 22.40 22.60 22.80 23.00 I ' 1 1 ' I 1 118 TPPH '■J'1"!........ I1 m/z 191.10 20.53%' mlz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192

5000 22.20 22.40 22.60 22.80 23.00 m/z 146.10 17.52% 96 165 1 29 39 51 63 74 83 l 115 126 139 152 I 176 [ 1 | । । । । | । । । I | I । । 1 p । P 1 [ i'ti 1 | । il!_| ’I 1 fl । ill I । 1 > 1 r | 1 1 1 > । 11 I 1 । 1 1 1 1 '| 1 r 1 1 | I 1 1 t | 1*t^l I | I I' I' I | I II'l |

n/z~> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80965: 2,5-Dihydrophosphole, 3-methyl-1 -oxo-1 -phenyl- 192 164 .... A... /. ■ । ' 1 1 1।1■'1 I 11 1 1 |i । । i । 22.20 22.40 22.60 22.80 23.00 5000 99 m/z 193.10 14.89% 115 47 77 177 I 67 125 146 2/ 38 TTTTUTTTT 157 , +Ml+r 444 134,,,1444155,, n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125849: Anthracene, 9-methyl- । । , । । । । । , 4 J । । । । । ! । L —। f— 192 22 20 22.40 22.60 22.80 23.00 m/z 96.00 13.52% 5000

96 165 28 39 51 63 74 83 J 105 115 126 139 152 J 176 /z-> TTTHIUTTTTTTTTHTTTTITTTTTTTHT ll—rr ' I r ' ' ' I ■ 1 ' 1 ' ' 1 1 .............. 1 1 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 | 22.20 22.40 22.60 22.80 23.00

9973.D 050102.M Tue May 07 15:52:03 2002 Page 18

NYC-WTC_000044047

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GCMS analysis results, sample AE09968, May 2002 · Box DEP Box 25

NYC-WTC_000043938

Gas chromatography-mass spectrometry analysis report for sample AE09968, detecting unknown compounds and 2,4-DDD surrogate with 78% recovery, dated May 9, 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996

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