GCMS analysis results for unknown compounds, sample AE10203, May 2002

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Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050802\10203 . D Vial: 21 Acq On 9 May 2002 7:42 am Operator: Mclean Sample 4/30 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 Phenanthrene, 9-methyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.36 ug/L 581119 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53- 2 2-Propenal, 3-(3,4-dimethoxyphen.. . 192 C11H1203 004497-40-9 42 3 Anthracene, 9-methyl- 192 C15H12 000779-02-2 49 4 Anthracene, 9-methyl- 192 C15H12 000779-02-2 40 Abundance Scan 3319 (22,580 min): 10203.D (-3312) (-) m/z 192.05 100.00% 192

5000 . ....... / 1 i 1 1 02 96 146 1 60

m/z-> 0 1 r 111 r 42 52 66 । J 118 | 7 I h I I | I i'i I | I II i | , fl-l-p H-I P I l'i I i 'i i i I i i I I] I I I I I i M i | i iTi I i i i I'p I i i I I i i I | I I I I |

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 4 22.20 22.40 22.60 22.80 23.00 m/z 191.10 22.41% Abundance #81033: Phenanthrene, 9-methyl- 192

5000 ........ ' i 1 1 ' 1 1 ■ ■ 1 1 ■ ' i ■ ■ । ■ i ■

22.20 22.40 22.60 22.80 23.00 m/z 193.10 15.87% 96 165

m/z-> 29 39 51 63 74 83 l 115 126 139 152 0 I J I I > r | 1 1 1 1 | 1 ■ 1 1 | 1 1 1 11110701 1 I'I» /I | Ilp 1 I I 1 | 1 r 1 1 | 1 1 1 | | 1 1 | 1 | I I I |'| I I I I |'| | | | | 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 176 l n rl* i 1 Ji I Abundance #80953: 2-Propenal, 3-(3,4-dimethoxyphenyl)- 192 161 22.20 22.40 22.60 22.80 23.00 5000 m/z 96.00 13.62% 77 121 149 177 91 103 52 64 138 0 1111" i1 ■" । n1 'A salsgan i''' 'i'1 .. I , I I I I I I I I I I I I I I I I I '’1 ’I — ■ I

n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125848: Anthracene, 9-methyl- 192 22.20 22.40 22.60 22.80 23.00 m/z 146.10 12.01%

5000

96 EE 27 39 51 63 82 I J 115 126 139 152 0 176 ------- 0 TR"—TmttTuhn v n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00

10203.D 050102.M Thu May 09 13:38:08 2002 Page 9

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