GCMS analysis results for unknown compounds, sample AE10203, May 2002

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Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10203 on May 10, 2002.

NYC-WTC_000044978–000044993

Folder label: “GCMS X 4/30/02 A 5/8/02”

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Data File C:\MSDCHEM\1\DATA\050802\10203.D Vial : 21 Acq On 9 May 2002 7:42 am Operator: Mclean Sample 4/30 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 23.11 0.66 ug/L 1071670 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 83 % 2 Phenanthrene-diO 188 C14D10 001517-22-2 72 / 3 Selenide, ethyl 1-methyl-l-pente... 188 C8H12Se 025128-48-7 58 4 2,2,9,9-Tetramethyldec-5-ene-3,7... 188 Cl4H20 102745-35-7 52 Abundance Scan 3409 (23.109 min): 10203.D (-3402) (-) m/z 188.10 100.00% 188

5000 ... ) 1 1 i 1 ■ 1 ' i ■ ■ 1 1 1 1 ■ ■ 1 i 1 1 ' 1 i

43 54 66 80 94 14A 160 22.80 23.00 23.20 23.40 132 0 —matut 146 44—— -HHH m/z 184.10 14.17% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/z 189.20 14.10% RR 80 94 160 17 30 42 52 00 J J 108 118 132 146 0 । । i ■ । i । i । > i । > । ' TTi । । । I I i । । i I I i pi" । H | I । i I | I I । । j t i r I । i । । I । rr ri TT i i । । । i I i । —1791794—— 11 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 ■ ■ । ' 1 11 ' 1 i 1 1 1 1 i 1 1 1 ' i 22.80 23.00 23.20 23.40 5000 m/z94.10 13.54%

80 94 160 | 30 42 52 66 108 118 132 146 1. 170179.1, |H 1 0-11 | ■ i । i i । I | i I । t | I i i i । I I I । । । I I I | I I rl I I I I | lli* ] ri i 11 । । । 11 PTTFpi 111 । । i i । । । tll’i । । । । । । । । । 14 Pl [ । TT‘ m/z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79821: Selenide, ethyl 1 -methyl-1 -penten-3-ynyl ---------------- 188 22.80 23.00 23.20 23.40 m/ z 80.05 10.09%

5000 1 79 159 11 „ 145 | 91 107 119 131 1 173

m/z-> 0 It1‘t1111t0P110B11IUOUTTTTTII‘T TUTUTuTTNT । "4 "4,, P TTl ... ..... .... 1 1 i 1 ' 1 ■ i ' 1 1 ■ r1 1 1 ' i 1 1 1 1 i 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

10203.D 050102.M Thu May 09 13:38:08 2002 Page 10

NYC-WTC_000044992

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