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GCMS analysis results, sample AE09969, May 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE09969 showing surrogate recovery and unknown compounds from May 9, 2002.

NYC-WTC_000043958–000043975

Folder label: “GCMS X 4/25/02 A 5/7/02

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NYC 9/11 Public Portal Document

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Data File C:\MSDCHEM\1\DATA\050602\9969.D Vial : 26 Acq On 7 May 2002 8:03 am Operator: Mclean Sample 4/25 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 8 Anthracene-dlO - Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.52 ug/L 568091 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d10- 188 C14D10 001719-06- 2 Phenanthrene-dlO 188 C14D10 001517-22- 90 3 Cycloheptanone, 4-phenyl- 188 C13H160 067688-28-2' 0 4 Antipyrine 188 C11H12N2O 000060-80-0 40 Abundance Scan 3409 (23.109 min): 9969.D (-3402) (-) m/z 188.10 100.00% 188

5000

94 1 ' I ' 1 1 ’ I 1 1 ' 1 I 80 . 160 , 22.80 23.00 23.20 23.40 43 57 66 . ,i 132 146 ||| |. mH i i'I i | I i i । 1 i । i । i r i i । i i i r | I i i 1 | r I i i i I | i i i | i i I | I i i i | i IT Tmn m/ Z 94.10 18.87% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 ' i 1 ' ■ 1 i 22.80 23.00 23.20 23.40 m/z 189.20 18.03% 80 94 160 , . 66 17 30 42 52 108 118 132 ' I I I I I I I I I t I I I I I I I I I I I I I I I 1111111,111 n 11 11 i । i i 111 i ,i । r 11 i i । 11 1464.179179 /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 1t8 1 1 i 1 । I 1 1 1 1 I ' 1 ' ' I 22.80 23.00 23.20 23.40 5000 m/ Z 80.10 14.08%

94 80 160 30 42 52 11I i ■ I ■108 66 118 > i132 146 , |,| 1 1170179,1,1 i i । i | I i | rri i 1 | 1 1 1 | I | I । । । i i i i । 14ffi 1'1 I" " I /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130_140 150 160 170 180 190 Abundance #79739: Cycloheptanone, 4-phenyl- 1 1 i ■ 1 ' 1 T 1?S 22.80 23.00 23.20 23.40 117 m/ z 184.10 104 13.84% 91 160 5000 131 170 27 3|9 51 65 78 145 111111111 , 111 I 11 lil । h m i'i, 1 " i" I " 1 "I ------------------- m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

9969.D 050102.M Tue May 07 15:48:36 2002 Page 11

NYC-WTC_000043973

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GCMS analysis results, sample AE09968, May 2002 · Box DEP Box 25

NYC-WTC_000043938

Gas chromatography-mass spectrometry analysis report for sample AE09968, detecting unknown compounds and 2,4-DDD surrogate with 78% recovery, dated May 9, 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998

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