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GCMS analysis results for sample AE09573, May 2002

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Laboratory report detailing gas chromatography mass spectrometry analysis of sample AE09573 conducted on May 14, 2002.

NYC-WTC_000023084–000023098

Folder label: “GCMS X 5/8/02 A 5/9/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050902\9572.D Vial: 9 Acq On 9 May 2002 9:48 pm Operator: Mclean Sample 5/8 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 5 Anthracene-dlO- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 23.11 0.53 ug/L 877563 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 90 2 Phenanthrene-diO 188 C14D10 001517-22-2 86 3 Cyclohept anone, 4 -phenyl- 188 C13H160 067688-28-2 50 4 Antipyrine 188 C11H12N2O 000060-80-0 40 Abundance Scan 3409 (23.109 min): 9572.D (-3403) (-) m/z 188.10 100.00% US

5000

80 94 160 0 22.80 23.00 23.20 23.40 43 57 66 118 132 146 , | 0 I " " I " 1 1 1 1 " 1 r’t I 1| ll >'| |H I l |‘i I I l'| I I'i l| I I I ! | I I I I | I I I I | II I i| Il I I | I I I I | I I " I I I I | I I I I | I1 TTT m/Z 189.10 16.46%I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 .............. ........................... , , , 22.80 23.00 23.20 23.40 m/ z 94.10 15.09% 80 94 16Q 66 17 30 42 52 0 TITTITTTTTTTTHT +10113 132146—179179/ 11 nfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 US IIIITSTII1"*III’II 22.80 23.00 23.20 23.40 5000 m/z 184.10 10.50%l

80 94 160 66 0 ■ i" " i * ■11 r — 108 118 ., 132.1146 , rl# . 179179 4 30 42 52 1. iz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79739: Cycloheptanone, 4-phenyl- 1(8 22.80 23.00 23.20 23.40 117 104 m/z 80.10 10.04%| 91 160 5000 131 170

m/z-> 0 111,, 111. 27 39 51 65 78 1 iiii , ,, mlgrl,7 ml i'i n Hll T-pT 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 + u .......................... .......................... 22.80 23.00 23.20 23.40

9572.D 050102.M Mon May 13 11:49:07 2002 Page 8

NYC-WTC_000023096

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