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GCMS analysis results for sample AE10898, May 21 2002

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Laboratory report detailing GCMS analysis of sample AE10898 conducted on May 21, 2002, including surrogate recovery data.

NYC-WTC_000024113–000024125

Folder label: “GCMS X 5/10/02 A 5/16/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\051602\10898.D Vial: 11 Acq On : 16 May 2002 10:41 pm Operator: Mclean Sample : 5/10 eh Inst : Instrumen Mise Multipl-r: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 4 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 23.11 0.45 ug/L 547274 Phenanthranene-dl0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d10- 188 C14D10 001719-06-8 78 2 Phenanthrene-diO 188 C14D10 001517-22-2 74 3 Antipyrine 188 C11H12N2O 000060-80-0 40 4 Cyclohept anone, 4 -phenyl- 188 C13H160 067688-28-2 37 Abundance Scan 3409 (23.109 min): 10898.D (-3403) (-) m/z 188.10 100.00% 188

5000

40 66 80 94 1 32 146 160 |।— 22.80 23.00 23.20 23.40 O1! [ " " p " I | I ! m/z 189.15 17.92% m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/ z 184.10 12.82% 17 30 42 52 66 ° 80 , 94 , 108118 132 146 160 170179 , i । II 0 1111111111 ■ 111" 11111111'1111111'' i111 ■' "111,1 .'I'" ~ ।' ।1' ]' 11 ] 1111111111111’l’l’ 11111lnp "‘I’ll’ ■ ■ ।. m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 m/ z 80.05 11.91%

80 94 160 30 42 52 66 108 118 132 146 I. 1701791,1 I 0 " " I" " I " 11 ■" I" ■ ■ I "4'l'|-i ■. i j.. ■ i ■■■■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79725: Antipyrine 18 8 22.80 23.00 23.20 23.40 96 m/ z 94.05 11.07% 5000 77 56 105 27 39 67 I, 115 130 145 159 173 n - 0 TIPTDTTT p-mmpm n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

10898.D 050102.M Fri May 17 15:06:52 2002 Page 7

NYC-WTC_000024124

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NYC-WTC_000024124Source: NYC Law Department, mirrored locally

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