GCMS sample analysis results, AE11903, June 3, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052202\11903.D Vial: 10 Acq On : 22 May 2002 9:09 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library- : C:\DATABASE\NIST98.L Peak Number 13 Anthracene-dlO- Concentration Rank 20 R.T. EstConc Area Relative to ISTD R.T. 23.07 0.27 ug/L 306264 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 188 C14D10 001719-06-8 95 2 Phenanthrene-diO 188 C14D10 001517-22-2 53 3 Antipyrine 188 C11H12N2O 000060-80-0 42 4 Benzene, 1-(1-cyclohexen-l-yl)-4... 188 C13H160 020758-60-5 42 Abundance Scan 3402 (23.068 min): 11903.D (-3395) (-) m/z 188.05 100.00% 188

5000

94 41 57 66 80 160 22.80 23.00 23.20 23.40 0-pmpT’- 1■ 1 m/z 94.10 18.85% iz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/z 189.10 17.81% 00 94 160 ,I 17 30 42 52 66 1 108118 ,132./146—*.,1791794 0 l1 "‘I'''' 11' -n-T* i. 111 lTTj« 11 > | > 11! f 1 > il ] ■ 11«। ‘i l»1 >11 ■ Uuur miz-> 10 2030405060 70 8090 100110120130140150160170180190 Abundance #79827: Phenanthrene-d10 1?®

22.80 23.00 23.20 23.40 5000 m/z 184.10 14.90%

80 94 160 42 52 66 30 0 ' 1 1 “ 11' '' 1 I' ' -HlThmmmmm 108118 132 146 ,,1.1 170179 tun miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #125688: Antipyrine .......................... ............. 188 22.80 23.00 23.20 23.40 96 m/z 187.10 12.80%

5000 77 56 105

n/z-> 0 mmH—tfar4l+H 27 39 । 68 115 129 145 159 173 *Trmm 11 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

11903.D 052202.M Tue May 28 12:07:51 2002 Page 16

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