GCMS calibration data for sample AE11931, May 2002

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Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052302\11931.D Vial: 11 Acq On : 23 May 2002 6:07 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 13 Anthracene-dlO- Concentration Rank 20

R.T. EstConc Area Relative to ISTD . R.T.

23.07 0.26 ug/L 236997 Phenanthranene-dl0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual )

1 Anthracene-dlO- 188 C14D10 001719-06-8 90) 2 Phenanthrene-diO 188 C14D10 001517-22-2 504/ 3 Antipyrine 188 C11H12N2O 000060-80-0 40 4 Benzene, 1-(1-cyclohexen-l-yl)-4... 188 C13H160 020758-60-5 40 Abundance Scan 3402 (23.068 min): 11931 .D (-3396) (-) m/z 188.15 100.00% 188

5000

94 66 80 160 22.80 23.00 23.20 23.40 40 m/z 94.10 21.42% a 1’1" m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/z 189.10 15.70% 80 94 160 , 17 30. 42 52 66 , J 108118 132 146 ,|.I 170179.|,i O 1PmPTHpt —t—mmmmnmm m/z-> 10 2030405060 70 8090 100110120 130140150160170180190 Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 m/ z 80.00 13.47%

94 80 160 30 42 52 66 11 108118 132 146 h. 170179,1 0-TITWTETTTTTTTTTTHTH titTT miz-> 10 20 30 40 50 60 70 80 90 100110120130140150 160170180190 Abundance #125690: Antipyrine 188 22.80 23.00 23.20 23.40 m/z 187.10 12.25% 96 5000 77 56 105 43 , 1

nfe-> 0 -LL 67 li .I i I 115 129 159 173 1 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 -------PPPPPP 22.80 23.00 23.20 23.40

11931.D 052202.M Wed May 29 09:51:03 2002 Page 16

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