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GCMS analysis results for sample AE10896, May 21 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS analysis of sample AE10896 conducted on May 21, 2002, including surrogate recovery data.

NYC-WTC_000024083–000024099

Folder label: “GCMS X 5/10/02 A 5/16/02

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Scanned page image, NYC-WTC_000024098
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\051602\10896.D Vial: 9 Acq On : 16 May 2002 9:03 pm Operator: Mclean Sample : 5/10 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.41 ug/L 433776 Phenanthranene- dl 0 22.95

Hit# Of 5 Tentative ID MW MolForm CAS# QUal

1 Anthracene-dl0- 188 C14D10 001719-06-8 86/ 2 Phenanthrene-diO 188 C14D10 001517-22-2 86—V 3 1,4-Naphthalenedione, 2-hydroxy-... 188 C11H8O3 000483-55-6 49 4 Antipyrine 188 C11H12N2O 000060-80-0 43 Abundance Scan 3409 (23,109 min): 10896.D (-3403) (-) m/z 188.10 100.00% US

5000 80 94 66 158 22.80 23.00 23.20 23.40 43 132 m/z-> 0 ‘ i1 " ' i'1111' "' i" " r 111 " r "' r 11' i ■ ■' ‘ 11' i " '11" 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 .. Ii""' m/ Z 80.05 24.89% Abundance #79826: Anthracene-d10- US

5000 22.80 23.00 23.20 23.40 m/ z 189.05 19.11% RR 80 94 160 , . 17 30 42 52 66 , 108118 132 146 ,|| 170179,i 0 mmmTITTTTTTH 11— m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 m/ z 94.00 18.74%

80 94 160 30 42 52 66 mfe-> 0 TWWTTTTTHTTTH +l 108 118 132 10.20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 46—+4179179— 146

Abundance #125707:1,4-Naphthalenedione, 2-hydroxy-3-methyl- /I 1 ' i ‘ 1 ■ ' T1 its 22.80 23.00 23.20 23.40 m/z 184.05 16.66%

5000

77- 105 131 160 50 , 115

/z-> 0 ... I1-1.. 11 ............ pi."'"I' • i “ ■11" 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 ii 1131" ]" >' l" !’3 ----- 22.80 23.00 23.20 23.40

10896.D 050102.M Fri May 17 15:04:58 2002 Page 11

NYC-WTC_000024098

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NYC-WTC_000024098Source: NYC Law Department, mirrored locally

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