NYC 9/11 Public Portal Document
Library Search Compound Report •
Data File : C:\MSDCHEM\1\DATA\051602\10896.D Vial: 9
Acq On : 16 May 2002 9:03 pm Operator: Mclean
Sample : 5/10 eh Inst : Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan
Library : C:\DATABASE\NIST98.L
*********************************************************************
Peak Number 7 4-Hydroxy-3,5-dimethylcinna ... Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
22.58 0.27 ug/L 282348 Phenanthranene-dl0 22.95
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 59
2 2,5-Dihydrophosphole, 3-methyl-l... 192 C11H13OP 1000196-97-5 59
3 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 59-
4 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 42
Abundance Scan 3319 (22.580 min): 10896. D (-3307) (-) m/z 192.10 100.00%|
192
5000
66
82 96 118 146 160 22.20 22.40 22.60 22.80 23.00
40
0 IT TH issjil......... . ..... 'I1'....... -p m/z 191.00 25.05%
m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200
Abundance #81030: 4-Hydroxy-3,5-dimethylcinnamic acid
192
5000
22.20 22.40 22.60 22.80 23.00
89 175 m/z 96.10 13.78%|
E 63 145
45 . I 77 1 105 117
Ot -444++H44,++ +TTHTTTTTTHT
135 | 163
m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200
Abundance #80965:2,5-Dihydrophosphole, 3-methyl-1-oxo-1-phenyl-
192
164
22.20 22.40 22.60 22.80 23.00
5000 99 m/z 193.10 12.58%|
115
47
67
77
125 146
177 h
0 —2738457, 4— 134,4155, H k
874lrll
miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200
Abundance #81033: Phenanthrene, 9-methyl- ■ i ‘ ■ i ■ ' ■ ■ i ' ■ ' 1 i ■ ■ "IT
192 22.20 22.40 22.60 22.80 23.00
m/z 146.10 11.94%
A
5000
96
iz->
29 39 51 63 74 83 j
0 ■ i ■ ■" i" "111" i "111''' " itTTfl ' i f >•] 111 ' r115 126 139 152
165
176
1" r " 111" rl " '11'1" 11 A 111 rhi i11
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200
l 22.20 22.40 22.60 22.80 23.00
10896.D 050102.M Fri May 17 15:04:54 2002 Page 10
NYC-WTC_000024097
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