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GCMS analysis results for sample AE11929, June 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11929 conducted on June 4, 2002.

NYC-WTC_000013524–000013550

Folder label: “GCMS X 5/22/02 A 5/23/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052302\11929.D Vial: 9 Acq On : 23 May 2002 4:29 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 13 2,5-Dihydrophosphole, 3-met... Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 22.54 0.27 ug/L 295707 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,5-Dihydrophosphole, 3-methyl-l... 192 C11H13OP 1000196-97-5 45 2 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 42 « 3 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 38 4 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 38 Abundance Scan 3312 (22.539 min): 11929.D (-3304) (-) m/z 192.10 100.00% 192

5000

82 96 146 160 1 A miz-> 44 66 Ot —mmmTHmmp 11111 “1' I" " I"'11 । I 118 I 2030405060 70 8090 100 110120 130140 150160 170 180190 200 l 22.20 22.40 22.60 22.80 m/z 191.10 21.82% Abundance #80965:2,5-Dihydrophosphole, 3-methyl-1-oxo-1-phenyl- 192 164

5000 99 ................................... fl, 115 22.20 22.40 22.60 22.80 ‘ ‘ ‘ 47 77 177 m/z 193.10 14.20% 67 125 146

miz-> 0 +27.39,4457,4++7H—lHlH+ 155, hordgomna/ h-rrp-r 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192 ■n-i-r-r-r-r-|-r-r 11**1*’’I 22.20 22.40 22.60 22.80 5000 m/z 146.00 13.46

96 29 39 51 63 74 83 115 126 139 152 165 176 | | 0 1!" TTDTTTTTTTTTTTTTTTTTHTT • ■ i ■ ■ miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80950:1,5-Naphthalenedithiole 192 ---A- 22.20 22.40 22.60 22.80 ‘ m/z 96.00 13.29 5000 115 128 159 40 57 69 79 96 147

miz-> 0 *h*h*mmmmmmmmmmmmm - —1177 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 • * i * * * * i * * 22.20 22.40 22.60 22.80

11929.D 052202.M Wed May 29 09:49:36 2002 Page 16

NYC-WTC_000013544

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NYC-WTC_000013544Source: NYC Law Department, mirrored locally

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