GCMS laboratory report for sample AE11908 detecting unknown compounds and 2,4-DDD on June 4, 2002.
NYC-WTC_000013014–000013042Folder label: “GCMS X 5-21-02 A 5-22-02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document ______________________ . Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052202\11908.D Vial: 15 Acq On : 23 May 2002 1:14 am Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C: \MSDCHEM\1\METHODS\050102 .M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 13 1,5-Naphthalenedithiole Concentration Rank 20 R.T. EstConc Area Relative to ISTD R.T. 22.54 0.25 ug/L 233616 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 59 2 2,5-Dihydrophosphole, 3-methyl-l... 192 C11H13OP 1000196-97-5/45 3 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 45 4 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H12O3 004497-40t© 42 Abundance Scan 3312 (22.539 min): 11908.D (-3300) (-) m/z 192.10 106.00% 192
5000 ...................... , "it r* * • • । ‘ 1 * * । T 96 146 160 22.20 22.40 22.60 22.80
niz-> 40 51 0 TTTTTTTTTTHT 70 82 ■ i11 ■ ■ i ■ ■ ■ ■ i ■" ■ i ■ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 L mHpp Hpr m/z 191.00 20.45 Abundance #80950:1,5-Naphthalenedithiole 19 2
5000 159 22.20 22.40 22.60 22.80 115 128 m/z 193.00 13.72 40 57 69 79 96 147 0- ! | ■ I 1,1 fl l r l . r l'.1! | trrlprrrptrePptrl r I | al-r - 111,111 • 1, 1 “i" ■ ■I1!... 17 iz-> 2030405060 70 8090 100 110120 130 140 150160 170 180190 200 Abundance #80965: 2,5-Dihydrophosphole, 3-methyl-1-oxo-1 -phenyl- 192 164 22.20 22.40 22.60 22.80 5000 99 m/z 146.00 12.28%| 115 47 77 177 67 07 125,2 146 27 38, 0!TT +87,+4l++,4r-44,H+.4+-+++++455, nayandyanur 1 ’ I *, n/z—> 2030405060 70 8090 100110120130140150160170180190200 Abundance #81030:4-Hydroxy-3,5-dimethylcinnamic acid 0/10/ 192 22.20 22.40 22.60 22.80 m/z 160.10 12.12% 5000
89 175 63 45 ,1 77 117 145 01 mH +4+4+44+4u4++195.Tptg ‘ 1 7 135 II, 163 , ............................./ miz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80
11908.D 052202.M Tue May 28 12.-15:45 2002 Page 16
NYC-WTC_000013034
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NYC-WTC_000012908
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11903.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012937
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11904.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012794
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11799.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012852
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11901.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012989
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11907.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013496
Laboratory report documenting GCMS analysis of sample AE11928 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012823
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11800.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012881
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11902.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013574
Laboratory report documenting GCMS analysis of sample AE11931 conducted on May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013524
Laboratory report documenting GCMS analysis of sample AE11929 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014578
Laboratory report showing GCMS analysis results for sample AE12534 including surrogate recovery data on June 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013968
GCMS analysis results for sample AE11603 dated June 4, 2002, documenting unknown compounds and surrogate recovery.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000012748
Department of Environmental Protection record of GCMS results generated in late May 2002.
Filed in the same folder
NYC-WTC_000012749
Administrative log recording sample identification, drip rates, and processing details for a GCMS batch.
Filed in the same folder
NYC-WTC_000012751
Gas chromatography-mass spectrometry blank analysis for sample AE11799 showing results below method reporting limits for semivolatile organic compounds, dated May 28, 2002.
Filed in the same folder
NYC-WTC_000012779
Calibration data for gas chromatography-mass spectrometry analysis of semivolatile organic compounds recorded on May 28, 2002.
Filed in the same folder
NYC-WTC_000012783
Reference standard analysis data for gas chromatography-mass spectrometry testing of semivolatile organic compounds on May 28, 2002.
Filed in the same folder