GCMS laboratory report for sample AE11908 detecting unknown compounds and 2,4-DDD on June 4, 2002.
NYC-WTC_000013014–000013042Folder label: “GCMS X 5-21-02 A 5-22-02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052202\11908.D Vial: 15 Acq On : 23 May 2002 1:14 am Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan "6 Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 14 1,1,1,5,7,7,7-Heptamethyl-3... Concentration Rank 17 R.T. EstConc Area Relative to ISTD R.T. 32.00 0.66 ug/L 421251 Chrysene-dl2 30.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,1,1,5,7,7,7-Heptamethyl-3,3-bi... 444 C13H40O5Si6 038147-00-1 38 2 Heptasiloxane, 1,1,3,3,5,5,7,7,9... 504 C14H44O6S17 019095-23-9 >37 3 1-Monolinoleoylglycerol trimethy. . . 498 C27H54O4Si2 054284-45-6 37 4 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-250 32 Abundance Scan 4922 (31.999 min): 11908.D (-4914) (-) m/z 73.10 0.00% 73 A 147 5000 221 281 355 - 429 31,60 31.80 32.00 32.20 32.40 40 96 1 1 0- ■ IT ' 1 111 1 ■ ■ i 1 ' i ■ ■ ■ ■ i ' m/z 147.10 65.76 nz-> 50 100 150 200 250 300 350 400 450 Abundance #26950:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)... 73 147 5000 267 355 429 31.60 31.80 32.00 32.20 32.40 45 207 m/z 221.10 50.47%| 0- ------------ ■ ■ I miz-> 50 100 150 200 250 300 350 400 450 Abundance #27374: Heptasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13-tet... 73 -------------------- 31.60 31.80 32.00 32.20 32.40 5000 207 m/z 281.10 29.26%
133 281 355
niz-> 0- 50 + 103 100 *i Pi 150 177 L t 2531 [ *’*’I1*’’/’***I’ 200 "I***I***I*’**I 250 300 3271 [ 377399 429 489 350 400 450 Abundance #27370: 1-Monolinoleoylglycerol trimethylsilyl ether i A 73 31.60 31.80 32.00 32.20 32.40 m/z 355.10 23.98 207 5000 147 34 103
n/z—> 0 50 ku 42 100 150 17744 r kd 200 +- _ 249, 250 281 [ 305327 355 325. 429 483 "1 .gal 1a 4T j’i 1 1 I ‘l Fi l i I 1—1- !*■ r I 300 350 400 450 31.60 31.80 32.00 32.20 32.40
11908.D 052202.M Tue May 28 12:15:48 2002 Page 17
NYC-WTC_000013035
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NYC-WTC_000012908
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11903.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012937
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11904.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012794
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11799.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012852
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11901.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012989
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11907.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013496
Laboratory report documenting GCMS analysis of sample AE11928 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012823
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11800.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012881
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11902.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013574
Laboratory report documenting GCMS analysis of sample AE11931 conducted on May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013524
Laboratory report documenting GCMS analysis of sample AE11929 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014578
Laboratory report showing GCMS analysis results for sample AE12534 including surrogate recovery data on June 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013968
GCMS analysis results for sample AE11603 dated June 4, 2002, documenting unknown compounds and surrogate recovery.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000012748
Department of Environmental Protection record of GCMS results generated in late May 2002.
Filed in the same folder
NYC-WTC_000012749
Administrative log recording sample identification, drip rates, and processing details for a GCMS batch.
Filed in the same folder
NYC-WTC_000012751
Gas chromatography-mass spectrometry blank analysis for sample AE11799 showing results below method reporting limits for semivolatile organic compounds, dated May 28, 2002.
Filed in the same folder
NYC-WTC_000012779
Calibration data for gas chromatography-mass spectrometry analysis of semivolatile organic compounds recorded on May 28, 2002.
Filed in the same folder
NYC-WTC_000012783
Reference standard analysis data for gas chromatography-mass spectrometry testing of semivolatile organic compounds on May 28, 2002.
Filed in the same folder