NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\1\DATA\052202\11799.D Vial: 6
Acq On : 22 May 2002 5:54 pm Operator: Mclean
Sample : 5/21 ad Inst : Instrumen
Mise : Multiplr: 1.00
MS Integration Params: LSCINT.e
2**
Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan
Library : C:\DATABASE\NIST98.L
*********************************************************************
Peak Number 14 1,1,1,5,7,7,7-Heptamethyl -3... Concentration Rank 14
R.T. EstConc Area Relative to ISTD R.T.
33.20 0.72 ug/L 399072 Perylene-dl2 34.66
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,1,1,5,7,7,7-Heptamethy1-3,3-bi. . . 444 C13H40O5Si6 038147-00-1 42
2 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25-0 38
3 3-Isopropoxy-1,1,1,7,7,7 -hexamet... 576 C18H5207Si7 071579-69-6 37
4 2,6-Dimethyl-3,4-bis(trimethylsi... 311 C15H29NO2Si2 1000079-52-1 25
Abundance Scan 5127 (33.203 min): 11799.D (-5115) (-) m/Z73.10 0.00%
73
147
221
5000
04 TTr
36
A 1
281
355
-| 429 1kT +
32.80 33.00 33.20 33.40 33.60
m/z 147.10 60.75%
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #26950:1,1,1,5,7,7.7-Heptamethyl-3,3-bis(trimethylsiloxy)...
73
5000
147
267
355 429
_Y
32.80 33.00 33.20 33.40 33.60
45 207 m/z 221.10 54.57%
niz->
O+ 1 ‘i
50
jund—mee
100 150 200 250 300 350 400 450 500 550
Abundance #87890:3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7...
147 221
73
-FT------
32.80 33.00 33.20 33.40 33.60
5000 m/z 281.00 33.35%
191
117 279
miz->
O+ TT
45
50
s. uL 2491..........
100 150 200 250 300 350 400 450 500 550
Abundance #26784:3-lsopropoxy-1.1,1,7,7,7-hexamethyl-3,5,5-tris(tri... AMAMAAAA4M4AA4AA,Aa
73 32.80 33'00 33.20 33.40 33.60
m/z 355.10 22.81%
5000,
147
43
n/z->
04 . 1
50
1 /
100 150
221
----- 519
281 327
T*r
561
200 250 300 350 400 450 500 550
415
M
32.80 33.00 33.20 33.40 33.60
11799.D 052202.M Tue May 28 12:03:01 2002 Page 17
NYC-WTC_000012815
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