NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\1\DATA\051402\10981.D Vial: 10
Acq On : 14 May 2002 8:50 pm Operator: Mclean
Sample : 5/10 kb Inst Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan
Library : C:\DATABASE\NIST98.L
*********************************************************************
Peak Number 12 1,1,1,5,7,7,7-Heptamethyl-3... Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
39.34 1.69 ug/L 1368580 Perylene-d12 34.71
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,1,1,5,7,7,7-Heptamethyl-3,3-bi... 444 C13H40O5Si6 038147-00-1 38
2 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25-0 38
3 Mercaptoacetic acid, bis(trimeth... 236 C8H20O2SSi2 0063 98 -62-5 37
4 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 22
Abundance Scan 6171 (39.338 min): 10981.D (-6152) (-) m/ z 73.05 /100.00%
73 147 221
5000 281
355
429
39.00 39.20 39.40 39.60
11 '1 ' +41L
O-T
40
-I
M. 4 , 193
' I 1
th, 4 I 325 I m/z 147.10 89.14%
m/z-> 0 50 100 150 200 250 300 350 400 _ /
Abundance #26950:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)...
73
147
5000 267 MAfi
355 429 39.00 39.20 39.40 39.60
45 207 m/z 221.10 85.87%
/z->
0—T
0 50
I
100 150 200 250 . 300 350
—L
400
Abundance #87890: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7...
147 2211
73 39.00 39.20 39.40 39.60
5000 m/z 281.00 48.58%
_
191
117 279
0—
45
TIT TTT
rh 1
’ i ■ '
249.........
m/z-> 0 50 100 150 200 250 300 350 400
Abundance #26922: Mercaptoacetic acid, bis(trimethylsilyl)-
73 39.00 39.20 39.40 39.60
147
m/z 207.00 44.24%
5000
45
_ 193
221
As
m/z->
0
13
I 1 1
0
l-
104
50 100
, 1 1691
150
, ,
200 250 300 350 400 3900 39.20 39.40 39.60
10981.D 050102.M Thu May 16 14:37:25 2002 Page 15
NYC-WTC_000023989
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