Gas chromatography-mass spectrometry blank analysis for sample AE11799 showing results below method reporting limits for semivolatile organic compounds, dated May 28, 2002.
NYC-WTC_000012751–000012778Folder label: “GCMS X 5-21-02 A 5-22-02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C: \MSDCHEM\ 1 \DATA\ 052202\521LB.D Vial: 3 Acq On : 22 May 2002 3:27 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************* * * ******************** * * Peak Number 17 Heptasiloxane, 1,1,3,3,5,5,... Concentration Rank 12
R.T. EstConc Area Relative to ISTD R.T.
35.38 0.57 ug/L 227136 Perylene-d12 34.66
Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Heptasiloxane, 1,1,3,3,5,5,7,7,9... 504 C14H4406Si7 019095-23-9 38 2 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25-0 35 3 2,6-Dimethyl-3,4-bis(trimethylsi ... 311 C15H29NO2Si2 1000079-52-1 35 4 Mercaptoacetic acid, bis(trimeth... 236 C8H20O2SSi2 006398-62-5 35 Abundance Scan 5497 (35.377 min): 521 LB.D (-5485) (-) m/ z 73.10 100.00% 73 A 147 221 «, M 5000 355 281 429 . ।M woo 3500 35.20 35.40 35.60 35.80 96
miz-> 0- 0 ■ ‘ 40 1 i 1 50 I 100 1 150 200 250 1, 300 1,....J...... I.... — 350 400 450 m/z 147.10 64.93% Abundance #27374: Heptasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13-tet... 73
A 5000 207 ‘dt ‘ ■ i ■ ■ ‘ ■ i ■ 3500 35.20 35.40 35.60 35.80 m/z 221.10 64.50% 133 281 355 0- —50L — 103 111771 150 +231 200 250 13274377399 300 350 400 429450 489 I"'' ■ IT nz-> 0 100 Abundance #87890:3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7... 147 221
73 35.00 35.20 35.40 35.60 35.80 5000 m/z 355.10 40.56% 191
iz-> 0- 0 45 1 '' 1 1 r 50 100 L 117
150 - . 1,242509.4.. 200 300 279
350 ■ 400 ■ i ■ ■ ■ ■ 450 i - ' ■ i ■ ■ ■ ■ i
Abundance #87845:2,6-Dimethyl-3,4-bis(trimethylsilyloxymethyl)pyridine 73 221 35.00 35.20 35.40 35.60 35.80 m/z 207.00 37.03%
5000 147
178 45 15 0- ।-I -i rrthr ....... 427120,1 ,, —— 266.296. ......... ............... n/z—> 0 50 100 150 200 250 300 350 400 450 35.00 35.20 35.40 35.60 35.80
521LB.D 052202.M Tue May 28 11:58:10 2002 Page 20
NYC-WTC_000012774
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NYC-WTC_000012823
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11800.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013496
Laboratory report documenting GCMS analysis of sample AE11928 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012852
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11901.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015496
Laboratory report showing non-detect levels of volatile organic compounds in a GCMS blank sample analyzed on June 5, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013524
Laboratory report documenting GCMS analysis of sample AE11929 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012794
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11799.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012908
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11903.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012989
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11907.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013574
Laboratory report documenting GCMS analysis of sample AE11931 conducted on May 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013418
Quality control document showing GCMS blank results for multiple volatile organic compounds analyzed on May 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012937
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11904.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025054
Laboratory report showing GCMS blank analysis for sample AE11379 conducted on May 21, 2002, with results below minimum reporting levels.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000012748
Department of Environmental Protection record of GCMS results generated in late May 2002.
Filed in the same folder
NYC-WTC_000012749
Administrative log recording sample identification, drip rates, and processing details for a GCMS batch.
Filed in the same folder
NYC-WTC_000012779
Calibration data for gas chromatography-mass spectrometry analysis of semivolatile organic compounds recorded on May 28, 2002.
Filed in the same folder
NYC-WTC_000012783
Reference standard analysis data for gas chromatography-mass spectrometry testing of semivolatile organic compounds on May 28, 2002.
Filed in the same folder
NYC-WTC_000012794
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11799.
Filed in the same folder