NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\l\DATA\052202\521LB.D Vial: 3
Acq On : 22 May 2002 3:27 pm Operator: Mclean
Sample : 5/21 ad Inst : Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan
Library : C:\DATABASE\NIST98.L
*********************************************************************
Peak Number 16 9H-Purin-6-amine, N-methyl-... Concentration Rank 11
R.T.. EstConc Area Relative to ISTD R.T.
35.03 0.58 ug/L 233266 Perylene-dl2 34.66
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 9H-Purin-6-amine, N-methyl-9-(tr... 221 C9H15N5Si 032865-83-1 9
2 Ethanone, 1-(2,3,4-trichlorophen... 222 C8H5C13O 013608-87-2 8
3 Benzene, 1,3,5-trichloro-2-(1-me... 222 C9H9C13 054965-70-79
4 2-Chloroaniline-5-sulfonic acid 207 C6H6C1NO3S 000098-36-2 5
Abundance Scan 5437 (35.025 min): 521 LB.D (-5435) (-) m/z 221.05
/ /100.00%
221
5000 96 133 430
40
' i ' *
73
0- i ■ ■ -r-T-r
191 264 ,295 34.60 34.80 35.00 35.20 35.40
m/z 207.00 53.45%
miz->
Abundance
50 100 150 200 250 300 350
#87924:9H-Purin-6-amine, N-methyl-9-(trimethylsily!)-
211
400
Jw“"W/—
73
5000
34.60 34.80 35.00 35.20 35.40
45 165 192 m/z 96.00 48.28%
miz->
0- .149,14 +4 it
50 100 150 200 250
1 1
300
• ■
350
• 1 i 1 1 ■ ■ 1 ■
400
Abundance #84879: Ethanone, 1-(2,3,4-trichlorophenyl)-
207
I "1,
43
34.60 34.80 35:00 35.20 35.40
5000 m/z 209.00 48.03%
74 181
109 143
15
0- 4 r 44 -+-*,h k — 4 228 ** * f • * * I I » I 1 1 1 * * * 1 l i
miz-> 50 100 150 200 250 300 350 400
Abundance #84887: Benzene, 1,35-trichloro-2-(1-methytethyl)-
207 34.60 34:80 35.00 35.20 35:40
m/z 133.00 45.57%
5000
136 171
0 15 1942+15 +41 228 ‘ । • f । • ■ * * । > * * * । * i ■ 1 ■ ■ i ■ * t • ' 1 । •
n/z—> 50 100 150 200 250 300 350 400 34.60 34.80 35.00 35.20 35.40
521LB.D 052202.M Tue May 28 11:58:10 2002 Page 19
NYC-WTC_000012773
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