GCMS analysis results for sample AE11928, June 2002

NYC 9/11 Public Portal Document • Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052302\11928.D Vial: 8 Acq On : 23 May 2002 3:40 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************* * * ********** Peak Number 19 3,6-Dioxa-2,4,5,7-tetrasila... Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T.

39.25 0.33 ug/L 167584 Perylene-d12 34.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25-0 43/ 2 2,6-Dimethyl-3,4-bis(trimethylsi... 311 C15H29NO2Si2 1000079-52-1 22 3 9H-Purin-6-amine, N-methyl-9-(tr... 221 C9H15N5Si 032865-83-1/9 4 2(1H)-Quinolinone, 4-phenyl- 221 C15H11NO 005855-57-2 5 Abundance Scan 6156 (39.249 min): 11928. D (-6143) (-) m/z 147.10 10/. 00% 1,7 221

73 5000 281 355 429 96 191 39.00 39.20 39.40 39.60 0' 40 | _ 1.......... | m/z 221.00 86.05% miz-> 50 100 150 200 250 300 350 400 Abundance #87890:3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7... 147 221

73 5000 ■ ■ i 1 ■ 1 • 1 1 1 39.00 39.20 39.40 39.60 191 m/ z 73.05 61.98% 117 45 A4 249 279 [ ■ i ■ ■ ■ ■ i ■ ' ■ ■ i ■

L 0- 1 1’1." r 1 ■ i r ■ T

niz-> 50 100 150 200 250 300 350 400 Abundance #87845:2,6-Dimethyl-3,4-bis(trimethylsilyloxymethyl)pyridine 73 Z!1 AAndpndpul 39.00 39.20 39.40 39.60 5000 147 m/z 207.00 39.81%

178 45 0- 15 1... * । T 1.92,-1204,4 4 Aj4 . 266 T—[—I—r-r-i—j—r

mfz~> 50 100 150 200 250 300 350 400 Abundance #87924:9H-Purin-6-amine, N-methyl-9-(trimethylsilyl)- 221 39.00 39'20 39'40 39.60 m/z 429.10 29.80% 73 5000 165 1?2 45 — 0 ■ ■ i ■ ■ ' ■ 1 ■ * i ■ ■ ■ ■ i ‘ 1 niz-> 50 100 150 200 250 300 350 400 39.00 39.20 39.40 39.60

11928.D 052202.M Wed May 29 09:48:59 2002 Page 22

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