GCMS calibration table data, sample AE10517, May 22, 2002

NYC 9/11 Public Portal Document Library Search compound Report Data File : C:\MSDCHEM\1\DATA\052102\10517.D Vial: 19 Acq On : 22 May 2002 4:00 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 17 3,6-Dioxa-2,4,5,7-tetrasila... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 39.25 1.21 ug/L 542979 Perylene-d12 34.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H30O2S14 004342-25-0/37 2 2,6-Dimethyl-3,4-bis(trimethylsi ... 311 C15H29NO2Si2 1000079-52/1 27 3 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 16 4 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47/3 16 Abundance Scan 6157 (39.255 min): 10517.D (-6142) (-) m/z 73.10 100.00%

Ju 73 147 221

5000 281 355 429 VYM

/z-> 0- 50 100 150 191 . —— 200 250 1.1 300 350 400 I 39.00 39.20 39.40 39.60 m/z 221.10 78.85% Abundance #87890:3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7... 147 21’1

73 A 5000 11 ■ 1 * ■ 39.00 39.20 39.40 39.60 191 m/z 147.10 77.90% 117 — . 279 45 th t 249_ 0- T‛1 ' 1 ■ i • ■ ’ ■■ i • • 1 ■ i ‘ ■ i ■ niz-> 50 100 150 200 250 . 300 350 400 Abundance #87845:2,6-Dimethyl-3,4-bis(trimethyIsiIyloxymethyl)pyridine 73 221 ___ ..** 39.00 39.20 39.40 39.60 50001 147 m/z 207.00 56.82% •I

0- 45 —rr 4924120,1 4 4 1,11266,286,.n... 15 ... 178 _top/woosu miz-> 50 100 150 200 250 300 350 400

wWCu Abundance #115144: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trim... 70 39.00 39.20 39-40 39.60 147 m/z 281.00 39.71%

5000 281 45 369 0 1 ■ i ' 117 207 1 249 ---I tnlz-> 50 100 150 200 250 300 350 400 39.00 39.20 39.40 39.60

10517.D 052202.M Wed May 22 11:48:35 2002 Page 2 0

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