GCMS calibration table data, sample AE10517, May 22, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052102\10517.D Vial: 19 Acq On : 22 May 2002 4:00 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 16 Cyclononasiloxane, octadeca... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 37.72 1.81 ug/L 811822 Perylene-d12 34.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclononasiloxane, octadecamethyl- 666 C18H5409Si9 000556-71-8 50 2 3,6-Dioxa-2,4,5,7-tetrasilaoctan. . . 294 C10H3002Si4 004342-25-0 /40 3 Mercaptoacetic acid, bis(trimeth... 236 C8H20O2SSi2 006398-62-5 33 4 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 27 Abundance Scan 5895 (37.716 min): 10517.D (-5883) (-) m/z 100/00% 73 147 221

5000 281 355 429 TTTPY 37.40 37.60 37.80 38.00 191 1 , 1 503 0 1 1 l i 1 ' 1 ‘ 4 ‘ - -------- m/z 147.10 88.99% /z-> 0 50 100 150 200250300350400450500550600650 Abundance #115158: Cyclononasiloxane, octadecamethyl- 73 147 221 429

355 5000 281 PTLTTITTOITTTT 37.40 37.60 37.80 38.00 m/z 221.10 75.29% —4 H 475 651 0- i ■ ■ ■ ■ ।111' i'1 • i • •»• i • — n/z-> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #87890:3,6-Dioxa-2,4,5,7-tetrasilaoctane; 2,2,4,4,5,5,7,7... ........ ....... .......... 147 221

73 37.40 37.60 37.80 38.00 5000 m/z 281.00 37.92% 191 _ 279 28, ----- 0 TTT — n/z-> 0 50 100 150 2(X) 250 300 350 400 450 500 550 600 650 Abundance #26922: Mercaptoacetic acid, bis(trimethylsilyl)- 73 37.40 37.60 37.80 38.00 147 m/z 207.00 34.81%

50001

0 713.1. 104 — 7__ 221 _A n/z-> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 37.40 37.60 37.80 38.00’11

10517.D 052202.M Wed May 22 11:48:33 2002 Page 19

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