GCMS laboratory report for sample AE11908 detecting unknown compounds and 2,4-DDD on June 4, 2002.
NYC-WTC_000013014–000013042Folder label: “GCMS X 5-21-02 A 5-22-02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052202\11908.D Vial: 15 Acq On : 23 May 2002 1:14 am Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan 15 Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 17 Cyclononasiloxane, octadeca... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 35.38 3.96 ug/L 1626260 Perylene-d12 34.66 Hit# of 5 Tentative ID MW MolForm CAS# Q 1 Cyclononasiloxane, octadecamethyl- 666 C18H5409Si9 000556-71-81 86 2 Mercaptoacetic acid, bis(trimeth... 236 C8H20O2SSi2 006398-62-5 38 3 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25/0 32 4 3-Isopropoxy-1,1,1,7,7,7 -hexamet... 576 C18H5207Si7 071579-69-6 32 Abundance Scan 5497 (35.377 min): 11908.D (-5486) (-) m/ z 73.10 100.00% 73 147 221 5000] 281 355 nmfRRrTr 429 35.00 35.20 35.40 35.60 35.80 191 Tl/Z-> 0- 40 1***’I***41 +t 0 50 100 mr Hr 399.1 ... ............... 150 200 250 300 350 400 450 500 550 600 650 m/z 147.10 72.74% Abundance #115158: Cyclononasiloxane, octadecamethyl- 73 147 221 429
355 5000 281 35.00 35.20 35.40 35.60 35.80 m/z 221.10 62.80%
niz-> 0- 1********* 050 100 150 200 m H 250 300 450 500 350 400 475 651 550 600 650 Abundance #26922: Mercaptoacetic acid, bis(trimethylsilyl)-
1l 73 147
□ 35.00 35.20 35.40 35.60 35.80 5000 m/z 280.95 31.16? 221 13 43. . 1C 0- T 0 104 1133 'i' 177 i111111 i ■ • • • j ■ > • ■ i ■ > miz-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #87890:3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7... 147 211 35.00 35.20 35.40 35.60 35.80 m/z 207.00 29.84% 73 _ 5000 191
n/z-> 0 28. I ■ 17■'! 1 0 50 —L 117
f l ux 279 i ■ ■ ■ ■ i ■'1 ■ i ■ • ■ ■ i 100 150 200 250 300 350 400 450 500 550 60) 650 35.00 35.20 35.40 35.60 35.80
11908.D 052202.M Tue May 28 12:15:54 2002 Page 20
NYC-WTC_000013038
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NYC-WTC_000012908
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11903.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012937
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11904.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012794
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11799.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012852
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11901.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012989
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11907.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013496
Laboratory report documenting GCMS analysis of sample AE11928 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012823
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11800.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012881
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11902.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013574
Laboratory report documenting GCMS analysis of sample AE11931 conducted on May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013524
Laboratory report documenting GCMS analysis of sample AE11929 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014578
Laboratory report showing GCMS analysis results for sample AE12534 including surrogate recovery data on June 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013968
GCMS analysis results for sample AE11603 dated June 4, 2002, documenting unknown compounds and surrogate recovery.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000012748
Department of Environmental Protection record of GCMS results generated in late May 2002.
Filed in the same folder
NYC-WTC_000012749
Administrative log recording sample identification, drip rates, and processing details for a GCMS batch.
Filed in the same folder
NYC-WTC_000012751
Gas chromatography-mass spectrometry blank analysis for sample AE11799 showing results below method reporting limits for semivolatile organic compounds, dated May 28, 2002.
Filed in the same folder
NYC-WTC_000012779
Calibration data for gas chromatography-mass spectrometry analysis of semivolatile organic compounds recorded on May 28, 2002.
Filed in the same folder
NYC-WTC_000012783
Reference standard analysis data for gas chromatography-mass spectrometry testing of semivolatile organic compounds on May 28, 2002.
Filed in the same folder