GCMS calibration table data, sample AE10517, May 22, 2002

Machine-extracted title · confidence 90%

Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.

NYC-WTC_000013285–000013308

Folder label: “GCMS X 5/21/02 A 5/21/02”

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NYC 9/11 Public Portal Document Library Search compound Report Data File : C:\MSDCHEM\1\DATA\052102\10517.D Vial: 19 Acq On : 22 May 2002 4:00 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 15 Cyclononasiloxane, octadeca... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

36.45 2.70 ug/L 1211980 Perylene-dl2 34.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclononasiloxane, octadecamethyl- 666 C18H5409Si9 000556-71-8 69 2 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25-0/38 3 Pentasiloxane, dodecamethyl- 384 C12H3604Si5 000141-63-9 35 4 Trisiloxane, 1,1,1,5,5,5-hexamet. . . 384 C12H3604Si5 003555-4773 35 Abundance Scan 5679 (36.447 min): 10517.D (-5670) (-) m/ z 73.10 100.00% 73 147 221

5000 281 355 429 36.20 36.40 36.60 36.80

miz-> 0-1 ■ irFr - - 191 50 100 150 200 250 4124 503 ‘ I ‘ 4 * ‘ 300 350 400 450 500 550 600 650 ' 1 ‘ ' I ‘ ‘ ‘ * i 1 ‘ 1 * I ' m/z 147.10 92.47% Abundance #115158: Cyclononasiloxane, octadecamethyl- 73 147 221 429

355 5000 281 ■■' 1 FI rr 1 ■ I ‘ 1 36.20 36.40 36.60 36.80 m/z 221.10 79.48% 475

miz-> 0- 11111111111 I.. 7... 1 1,4.011/0 50 100 150 200 250 300 350 400 . 450 500 550 600 ■ ■ i ■ ■ ‘ ■ i' 651 650 Abundance #87890:3,6-Dioxa-2,4,5,7-tetrasiIaoctane, 2,2,4,4,5,5,7,7... 147 221 • • i • • 11 73 36.20 36.40 36.60 36.80 5000 39.21% 191

niz-> Abundance 28. 0- ■ 1 '‘i s-r 50 100 L 117 — • 250 279 | • i • 1 • i • ■ • ■ i ‘ । ■ i ■ • • > i • 150 200 250 300 350 400 450 500 550 600 650 #115143: Pentasiloxane, dodecamethyl- 1 • j > » > • l i > 1 » j > i

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73 147 281 36.20 36.40 36.60 36.80 m/z 355.10 33.22% 5000 369 207 117 tr, - 0 —33 177, 1 249. Mi fir i-i | A Pr < > 11 f । ’ I1+’41*4**I****1***’1:*’’144 ■ • i ■ ■ ■ i ■ ■ m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 36.20 36.40 36.60 36.80

10517.D 052202.M Wed May 22 11:48:31 2002 Page 18

NYC-WTC_000013305

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