GCMS analysis report sample AE11908, June 4, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052202\11908.D Vial: 15 Acq On : 23 May 2002 1:14 am Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise • Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan *f Library- : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 19 Cyclononasiloxane, octadeca... Concentration Rank 5 R.T., EstConc Area Relative to ISTD R.T. 37.71 2.56 ug/L 1053280 Perylene-dl2 34.66 Hit# of 5 Tentative ID MW MolForm CAS# Q 1 Cyclononasiloxane, octadecamethyl- 666 C18H5409Si9 000556-71-6 91 2 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25-0 40 3 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 35 4 Pentasiloxane, dodecamethyl- 384 C12H3604Si5 000141-63-9 35 Abundance Scan 5894 (37.710 min): 11908.D (-5879) (-) m/z 73.05 100.00% 73 147 221

5000 281 355 429 PTP • । ■ ■ ■ ■ । ‘ । ■ ■ ■ ■ । 191 503 37.40 37.60 37.80 38.00 1 — — 0- > 'I' ' - • ■ i ■ ‘ ‘ i • m/z 147.10 91.83% mfe-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #115158: Cyclononasiloxane, octadecamethyl- 73 147 221 429

355 50001 281 .. Ti ■ in Af. 37.40 37.60 37.80 38.00 m/z 221.10 83.44% 475 miz-> 0- 1 ' 1 I ’ 1 1 111 1 -- JLH 50 100 150 200 250 300 350 400 450 500 550 600 650 — 651

Abundance #87890:3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5.5,7,7... 147 221

73 37.40 37.60 37.80 38.00 5000 m/z 281.00 38.79% 191 117 279 28, . 1 250 | niz-> 01 • • '11444/1/4

Abundance I' " ■ ■ if ■ i ■ ■' ■ i 1 ■ ■ ■ i ■ ‘ 50 100 150 200250300350400450500550600650 ■ i ■ ■' ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i •'1 ■ i ■'

#26961: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trime... • • i • W Up 11——1 73 147 37.40 37.60 37.80 38.00 m/z 355.00 35.77% 281 5000

369

n/z-> o1 244+ 50 117177227 249, 1*71 Pr Ppt PPpt 100 338 1 150 200 250 300 350 400 450 500 550 600 650 37.40 37.60 37.80 38.00

11908.D 052202.M Tue May 28 12:15:57 2002 Page 22

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