GCMS analysis results, sample AE09154, May 2002

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Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\050902\9154.D Vial: 19 Acq On : 10 May 2002 6:47 am Operator: Mclean Sample : 5/8 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 14 Cyclononasiloxane, octadeca... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

35.42 4.20 ug/L 2482770 Perylene-dl2 34.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclononasiloxane, octadecamethyl- 666 C18H5409Si9 000556-71-8 91 2 1,1,1,5,7,7,7-Heptamethyl-3,3-bi... 444 C13H40O5Si6 038147-00-150 3 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25-0 50 4 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 38 Abundance Scan 5504 (35.418 min): 9154.D (-5492) (-) m/ z 73.10 100.00% 73 147 221

5000 281 355 429 35.00 35.20 35.40 35.60 35.80

m/z-> 43 117 0- TTTT TIPuT 191 50 100 150 200 4 1, 4 32541. 499— — 250 300 350 400 450 500 550 600 650 503 m/z 147.10 81.34% Abundance #115158: Cyclononasiloxane, octadecamethyl- 73 147 221 429

355 ----- 5000 281 i 1 ' 1 ■ i 35.00 35.20 35.40 35.60 35.80 m/z 221.10 68.32% 475

n/z-> 0- 50 100 150 200 250 300 350 alaapom 400 450 500 PIIIII/ r 550 600 651 650 Abundance #26950:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)... 73 I 1 ' 1 1 i 1 ' p=mre i ’ ।-i-■ 147 35.00 35.20 35.40 35.60 35.80 5000 267 m/ Z 281.00 34.47% 355 429 207

0- n/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #87890:3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7... 118 ' ■ i ■ ■ ' ■ i ' 1 ■ ' i ■ ' 147 221 35.00 35.20 35.40 35.60 35.80 m/z 355.10 29.39% 73 5000 191 ___ ।_ ,_ _______________________ _______ __ j i j 117 279 0 28 , । L 250 J.......................... /z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 35.00 35.20 35.40 35.60 35.80

9154.D 050102.M Mon May 13 11:29:00 2002 Page 17

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