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GCMS analysis results for sample AE11384, May 22 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE11384 conducted on May 22, 2002.

NYC-WTC_000025163–000025181

Folder label: “GCMS X 5/15/02 A 5/17/02

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Scanned page image, NYC-WTC_000025179
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\051702\11383.D Vial: 10 Acq On : 17 May 2002 8:07 pm Operator: Mclean Sample : 5/15 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 9 3-Phenyl-4,5-dimethyl-2,1-o.. Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T. 34.93 0.25 ug/L 225052 Perylene-dl2 34.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Phenyl-4,5-dimethyl-2,1-oxabor... 202 C13H19BO 1000062-26-1/25 2 Benzene, (2-methyl-1-methylenebu... 160 C12H16 026452-86-8/9 3 IH-Benzimidazole, 2-methyl- 132 C8H8N2 000615-15-6 5 4 Benzofuran, 7-methyl- 132 C9H80 017059-5248 5 Abundance Scan 5421 (34.931 min): 11383.D (-5419) (-) m/z 132.30 100.00% 132

5000 44 207 96 116 261 73

281 34.60 34.80 35.00 35.20 Of ■ i ' 1 ' ' i ■ ■ i ■1 ■ ■ i ■' 11.8 p ■ | i 1 ‘ * * ■ ! ' ‘ | 1 1 ‘ I ' ' ' ‘ I ' ' —L m/z 131.60 63.98% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #59360: 3-Phenyl-4,5-dimethyl-2,1 -oxaborolane 131

5000 146 34.60 34.80 35.00 35.20 91 m/z 129.20 47.89% 117 29 53 68 m/z-> 20 0 40 +— 4 , 103 189202 ■ i ' ■ 1 1 । 1 1 ■ 1 । 1 1 1 ■ । ■ . . . । . . . . । . 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #59712: Benzene, (2-methyl-1-methylenebutyl)- 132 91 .ATMA4.A...... 103 34.60 34.80 35.00 35.20 5000 117 m/z 207.00 . 47.89% 77 51 145 160

m/z—> 0 20 27 h

40 i 65 I

60 80 100 120 140 160 180 200 220 240 260 280 9 Abundance #122087:1 H-Benzimidazole, 2-methyl- ■ ' i ' ' 132 34.60 34.80 35.00 35.20 m/Z 116.00 42.25%

5000

63 77 91 104118

m/z-> ' 0 ’14111114’’ । । 11 1 । ■ 20 40 LL i II III i ill 11

60 80 100 120 ' | - ' ' ' ! ■ ' ■ • l ' - ■ ' | 140 160 180 200 । 220 | ‘ 240 260 280 34.60 34.80 35.00 35.20

11383.D 050102.M Tue May 21 11:55:35 2002 Page 12

NYC-WTC_000025179

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NYC-WTC_000025179Source: NYC Law Department, mirrored locally

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