Laboratory report showing GCMS analysis results for sample AE11384 conducted on May 22, 2002.
NYC-WTC_000025163–000025181Folder label: “GCMS X 5/15/02 A 5/17/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\051702\11383.D Vial: 10 Acq On : 17 May 2002 8:07 pm Operator: Mclean Sample : 5/15 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 2-Methyl-8-trifluoromethyl-... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 31.38 0.24 ug/L 283019 Chrysene-dl2 30.81 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Methyl-8-trifluoromethyl-4[1H]... 227 C11H8F3N0 1000227-02-8 22 2 Silicic acid (H6-Si2-07), hexame... 258 C6H1807Si2 004371-91-9 12 3 Silicic acid (H6-Si2-O7), hexame... 258 C6H1807Si2 004371-91-9/12 4 Phthalic acid, diisooctyl ester 390 C24H3804 001330-91-2 10 Abundance Scan 4817 (31.382 min): 11383.D (-4810) (-) m/z 227.10 100.00% 227 149
5000 57 113 69 85 99 167 41 198 240 31.00 31.20 31.40 31.60 31.80 0 I’’’ I ' 1 1 1 i ' ■" ■ I T-r-n-r-r-r-p-r-r-r-]-r-r-r-r-p- — m/z 149.10 70.19% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #89109: 2-Methyl-8-trifluoromethyl-4[1 H]quinolone 179 207 227
5000 MA 31.00 31.20 31.40 31.60 31.80 69 89 129 ! 158 m/z 113.50 44.38% .... 41 52 41,4102114 1140,'I papii" ■ 1921 j 0 I 1111 I 1 1 1 1 I।''। I 11,1 I '| । ' I 11 1 ' I । 11 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #127067: Silicic acid (H6-Si2-07), hexamethyl ester 227 ■ - i ■ ■ 31.00 31.20 31.40 31.60 31.80 5000 196 m/z 57.10 42.46%
167 31 45 59 77 91 107 121 137 151 | ,181 I II, , 213 | I1 , , i , , ,258 0 *i , , A mfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #89125: Silicic acid (H6-Si2-07), hexamethyl ester TIT 227 31.00 31.20 31.40 31.60 31.80 m/ z 49.10 25.06% 197 5000 167 4 m/z--> 45 61 _ 91 77, 1 107 121 137 1511 0 1 1 1 ' I ''1 1 1 1* 1 1 1 1 1I 11'1 . . 20 40 60 80 100 120 140 — „* 181 L 160 180 200li , 213220 240 260 1 1 1 ' 1 1 ' 1 1 i 1 1 ' 31.00 31.20 31.40 31.60 31.80 i' 1
11383.D 050102.M Tue May 21 11:55:32 2002 Page 11
NYC-WTC_000025178
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NYC-WTC_000025145
Laboratory report showing GCMS analysis results for sample AE11383 conducted on May 22, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023904
Laboratory report showing GC/MS analysis of sample AE10981 with surrogate recovery data for 2,4-DDD.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022763
GCMS analytical report for environmental sample AE09331 including surrogate compound data from May 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024014
Laboratory report showing GC/MS analysis of sample AE10985 with surrogate recovery data for 2,4-DDD.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024083
Laboratory report detailing GCMS analysis of sample AE10896 conducted on May 21, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022886
GCMS analytical report for environmental sample AE09332 including surrogate compound data from May 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023439
Laboratory report showing GC/MS analysis results for sample AE10137 including surrogate recovery data on May 14, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045171
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10308 conducted on May 17, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045624
Laboratory report detailing GC/MS analysis of sample AE10606 including surrogate recovery data in May 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044885
Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10198 on May 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045155
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10307 conducted on May 17, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043938
Gas chromatography-mass spectrometry analysis report for sample AE09968, detecting unknown compounds and 2,4-DDD surrogate with 78% recovery, dated May 9, 2002.
1 shared topics · similarity 0.996
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NYC-WTC_000025051
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
Filed in the same folder
NYC-WTC_000025052
Fragmented document containing GCMS calibration slope information for the period of May 15 to May 17, 2002.
Filed in the same folder
NYC-WTC_000025054
Laboratory report showing GCMS blank analysis for sample AE11379 conducted on May 21, 2002, with results below minimum reporting levels.
Filed in the same folder
NYC-WTC_000025072
Calibration report for GCMS analysis of sample AE11379 performed on May 21, 2002, listing response factors for target analytes.
Filed in the same folder
NYC-WTC_000025076
Laboratory report documenting GCMS calibration verification for sample AE11379 conducted on May 20, 2002, listing specific compound concentrations.
Filed in the same folder