NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\l\DATA\052202\11903.D Vial: 10
Acq On : 22 May 2002 9:09 pm Operator: Mclean
Sample : 5/21 ad Inst : Instrumen
Mise : Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan 75
Library- : C:\DATABASE\NIST98.L
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Peak Number 14 1,1,1,5,7,7,7-Heptamethyl-3... Concentration Rank 18
R.T. EstConc Area Relative to ISTD R.T.
32.00 0.37 ug/L 308426 Chrysene-dl 2 30.76
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 l,l,l,5,7,7,7-Heptamethyl-3,3-bi... 444 C13H40O5Si6 038147-00-1 477
2 Mercaptoacetic acid, bis(trimeth... 236 C8H20O2SSi2 006398-62-5 38
3 2-(2,6,6-Trimethylcyclohex-l-eny... 222 C14H22O2 1000185-64-1 22
4 Octasiloxane, 1,1,3,3,5,5,7,7,9,... 578 C16H50O7Si8 019095-24/0 17
Abundance Scan 4922 (31.999 min): 11903.D (-4914) (-) m/ z 73.10 100.00%
73
147
5000 221
281 355
429 31.60 31.80 32.00 32.20 32.40
40 —
0-r 1’1"
II
m/z 147.10 60.95%
miz-> o 50 100 150 200 250 300 350 400
Abundance #26950:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)...
73
147 .................. ,.........................
5000 267
355 429 31.60 31.80 32.00 32.20 32.40
45 207 m/z 221.10 48.34%
0- .......... Ill............. .................................
i ■ ■ ■ ' i ' • ' ■ i ■ ■ ■ ' i 1 1 tir 1 1 ' r1 1
1...................
1 i ■ ■ ■
1. i ■ 1 ■ i
—
m/z-> 0 50 100 150 200 250 300 350 400
Abundance #26922: Mercaptoacetic acid, bis(trimethylsily!)-
73
147 11....
31.60 31.80 32.00 32.20 32.40
5000 m/z 207.00 28.48%
221
45
__ 193
. 13
0- r , l 11, 104
' 1T IT r 1 f r1'
169 1
iz-> 0 50 100 150 200 250 300 350 400
Abundance #66034:2-(2,6,6-T rimethylcyclohex-1 -enyl)cyclopropanecarb...
147 31.60 31.80 32.00 32.20 32.40
m/z 281.00 27.10%
107
5000 175 207
41 79
4.
0
m/z—> 0 50 100 150 200 250 300 350 400 31.60 31.80 32.00 32.20 32.40
11903.D 052202.M Tue May 28 12:07:53 2002 Page 17
NYC-WTC_000012929
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