GCMS calibration table data, sample AE10517, May 22, 2002

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Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.

NYC-WTC_000013285–000013308

Folder label: “GCMS X 5/21/02 A 5/21/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C: \MSDCHEM\1\DATA\052102\10517.D Vial: 19 Acq On : 22 May 2002 4:00 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 11 1,1,1,5,7,7,7-Heptamethyl-3... Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

32.00 0.48 ug/L 340704 Chrysene-dl2 30.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,1,1,5,7,7,7-Heptamethyl-3,3-bi... 444 C13H40O5Si6 038147-00-1 37 2 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25-0 37 3 1-Monolinoleoylglycerol trimethy... 498 C27H54O4Si2 054284-45-6 37 4 2,6-Dimethyl-3,4-bis(trimethylsi ... 311 C15H29NO2Si2 1000079-52/1 32 Abundance Scan 4922 (31.999 min): 10517.D (-4911) (-) m/z 73.10 100.00% 73

147 221 5000

4.11k 281 355 429 .... ly..... 31.60 31.80 32.00 32.20 32.40

miz-> 0- 49 50 100 150 200 250 300 350 400 I ■ ■ i • ■ ■ • i ■ ■ b 450 m/z 147.00 62.46% Abundance #26950:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiIoxy)... 73 147 5000 267 355 429 31.60 31.80 32.00 32.20 32.40 45 207 m/z 221.10 59.04% 0 • • i ■ ■ ■ ■ i • ■ ■ ■ i • ■ ■ ' i ■ ■ • ■ i ‘ ‘ • ■ i ■ ■ ' ■ i ■ ‘ 1 1 i ' ■ 1 ■ 1 ■ • ' ■ i miz-> 50 100 150 200 250 300- 350 400 450 Abundance #87890:3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7... 147 2!1

73 31.60 31.80 32.00 32.20 32.40 5000 m/z 281.00 29.97% 191 117 279 45 - .. 1 249 L 0- '' 1' I n r ■ i ■ r • i • 1 ■ ■ I ■ ■ 1 1 I ' ■ 1 ■ i ■ ■ ■ ■ i niz-> 50 100 150 200 250 300 350 400 450 Abundance #27370:1-Monolinoleoylgiycerol trimethylsilyl ether 1.8 114 73 31.60 31.80 32.00 32.20 32.40 m/z 206.95 25.71% 207 5000 147 34 103 281 WWtwA” 0 444 4 4 + 124 77+ +.249, 249 T 117’ .305327,355 114 T 325. 429 483 ■ । I 1 ' ' ' I 1 ' iz-> 50 100 150 200 .250 300 350 400 450 31.60 31.80 32.00 32.20 32.40

10517.D 052202.M Wed May 22 11:48:23 2002 Page 14

NYC-WTC_000013301

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